Influence of Drying Parameters and Methods of Fractionation in the Chemical Composition of Dehydrated Ginger (Zingiber Officinale Roscoe)

Cristian José Cristofel, Cláudia Moreira Santa Catharina Weis, Giovanna Camile Vaz Goncalves, Helen Treichel, L. Bertan, Luciano Tormen
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Abstract

Ginger is widely commercialized in the food, chemical, and pharmaceutical industries, mainly in dehydrated and powdered form. To do this, the raw material must go through a drying process, which can significantly influence its characteristics. This study proposed to investigate the ginger dehydration process under three different fractionation methods: whole, sliced, and grated, and subjected to three other drying processes: oven with forced air circulation and renewal (CC) and without forced air circulation and regeneration (SC), both for temperatures of 50, 60, 70 and 80 °C, and freeze-drying. The data obtained allowed the construction of drying curves depending on time. The samples were analyzed for color, phenolic compounds, substances reactive to thiobarbituric acid (TBARS), acidity titratable capacity, 2,2-Diphenyl-1-picrylhydrazyl (DPPH) radical scavenging capacity, and chemical composition of the oils essential, obtained by hydrodistillation. The ginger drying kinetics shows that the process efficiency is maximized by combining parameters such as more significant sample fractionation, high temperatures, and forced air circulation. Notably, the preservation of bioactive compounds is more effective under conditions of lower temperature, lower fractionation, and absence of forced air circulation, highlighting the importance of these factors in maintaining the nutritional properties of ginger. The evaluation of the essential oil reinforces the need for appropriate strategies, such as freeze-drying or drying in an oven with forced air circulation at 50 °C, to minimize the degradation of volatile components, contributing to optimizing ginger dehydration processes promoting and preserving its nutritional and functional benefits.
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干燥参数和分馏方法对脱水生姜化学成分的影响
生姜主要以脱水和粉末形式广泛用于食品、化工和制药行业。为此,原料必须经过干燥过程,而干燥过程会极大地影响原料的特性。本研究建议调查生姜在三种不同的分馏方法下的脱水过程:整块、切片和磨碎,以及其他三种干燥过程:带强制空气循环和再生(CC)和不带强制空气循环和再生(SC)的烘箱(温度均为 50、60、70 和 80 °C),以及冷冻干燥。根据所获得的数据,可以绘制出不同时间的干燥曲线。对样品的颜色、酚类化合物、硫代巴比妥酸活性物质(TBARS)、酸度滴定容量、2,2-二苯基-1-苦基肼(DPPH)自由基清除能力以及通过水蒸馏获得的精油化学成分进行了分析。生姜干燥动力学表明,通过结合更显著的样品分馏、高温和强制空气循环等参数,可以最大限度地提高工艺效率。值得注意的是,在温度较低、分馏程度较低、无强制空气循环的条件下,生物活性化合物的保存更为有效,这凸显了这些因素在保持生姜营养特性方面的重要性。对精油的评估加强了采取适当策略的必要性,如冷冻干燥或在 50 °C 强制空气循环烘箱中干燥,以最大限度地减少挥发性成分的降解,从而有助于优化生姜脱水工艺,促进和保存其营养和功能性益处。
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