Template Synthesis of SnO2 Hollow Microspheres and Enhanced Photocatalytic Activity

IF 0.9 4区 材料科学 Science of Advanced Materials Pub Date : 2024-04-01 DOI:10.1166/sam.2024.4655
Kai Du, Jiao Yang, Gaojie Li, Yapeng Li, Zewen Gan
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Abstract

The paper describes a methodology for fabricating hollow microspheres of tin dioxide by utilizing carbonaceous saccharide microspheres as templates. The fabricated SnO2 microspheres exhibit uniform morphology and high crystallinity, which were verified with X-ray diffraction analyses and electron microscopy images. Through controlling different solvent and heating rate, we can accurately control the uniformity, dispersion and surface morphology of the hollow microspheres. Additionally, the study explored the utilization of the prepared SnO2 hollow microspheres and SnO2 nanoparticles in the degradation of Rhodamine B as detected by ultraviolet ray. Test data results indicated that the photocatalytic efficiency of SnO2 hollow microspheres surpassed that of the nanoparticles, attributed to the former’s multi-level reflection of light, resulting in effective light utilization. The hollow SnO2 microspheres can serve as an excellent candidate for a photocatalyst, and this controllable yet sample synthesis route is anticipated to be employed for production of numerous hollow metal oxide structures with superior photoelectric properties.
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模板合成二氧化锡空心微球并增强其光催化活性
本文介绍了一种以碳糖微球为模板制造二氧化锡空心微球的方法。经 X 射线衍射分析和电子显微镜图像验证,制备的二氧化锡微球形态均匀、结晶度高。通过控制不同的溶剂和加热速率,我们可以精确地控制空心微球的均匀性、分散性和表面形貌。此外,研究还探讨了制备的二氧化锡空心微球和二氧化锡纳米粒子在紫外线检测罗丹明 B 降解中的应用。测试数据结果表明,二氧化锡空心微球的光催化效率超过了纳米粒子,这是因为前者能对光进行多级反射,从而有效地利用了光。二氧化锡空心微球可作为光催化剂的理想候选材料,这种可控的样品合成路线有望用于生产多种具有优异光电性能的空心金属氧化物结构。
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来源期刊
Science of Advanced Materials
Science of Advanced Materials NANOSCIENCE & NANOTECHNOLOGY-MATERIALS SCIENCE, MULTIDISCIPLINARY
自引率
11.10%
发文量
98
审稿时长
4.4 months
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