Effect of sodium hydroxide treatment on the fracture toughness of luffa natural fiber reinforced epoxy epikote 828

IF 1.3 Q3 CHEMISTRY, MULTIDISCIPLINARY Vietnam Journal of Chemistry Pub Date : 2024-05-10 DOI:10.1002/vjch.202400010
D. Trung, Doan Thi Yen Oanh
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Abstract

Micro‐sized luffa natural fibers (MLNFs) were derived from raw luffa natural fibers from Vietnam by undergoing treatment with sodium hydroxide. This study examined the impact of sodium hydroxide concentration, temperature, and treatment duration on the fracture toughness of epoxy resin 828 reinforced with MLNFs. The results showed that the fracture toughness of the composite, as measured by the critical‐stress‐intensity factor (KIC) and Izod impact strength, was improved after the treatment of the MLNFs with sodium hydroxide. Specifically, with the optimal sodium hydroxide treatment parameters of 6% NaOH at 70 °C for 6 h, the critical‐stress‐intensity factor increased by 93% (from 2.0 to 3.86 MPa m1/2) and the Izod impact strength rose by 44.6% (from 3.81 to 5.51 kJ/m2). The thermal properties and surface structure of MLNFs treated with NaOH were analyzed using thermogravimetric analysis (TGA) and scanning electron microscopy (SEM) images.
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氢氧化钠处理对丝瓜天然纤维增强环氧树脂 epikote 828 断裂韧度的影响
微尺寸丝瓜天然纤维(MLNFs)是从越南的丝瓜天然纤维原料中通过氢氧化钠处理提取出来的。本研究考察了氢氧化钠浓度、温度和处理时间对用 MLNFs 增强的环氧树脂 828 断裂韧度的影响。结果表明,用氢氧化钠处理 MLNFs 后,以临界应力强度因子(KIC)和伊佐德冲击强度衡量的复合材料断裂韧性得到了改善。具体来说,最佳氢氧化钠处理参数为 6% NaOH 70 °C 6 小时,临界应力强度因子提高了 93%(从 2.0 兆帕 m1/2 提高到 3.86 兆帕 m1/2),伊佐德冲击强度提高了 44.6%(从 3.81 kJ/m2 提高到 5.51 kJ/m2)。利用热重分析 (TGA) 和扫描电子显微镜 (SEM) 图像分析了经 NaOH 处理的 MLNFs 的热性能和表面结构。
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来源期刊
Vietnam Journal of Chemistry
Vietnam Journal of Chemistry CHEMISTRY, MULTIDISCIPLINARY-
CiteScore
1.70
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