Production of Synthetic Carbonate Rocks Using Limestone Mining Waste: Mineralogical, Petrophysical and Geomechanical Characterization

Yago Ryan Pinheiro dos Santos, Igor Gomes, Analice Lima, J. Barbosa, Osvaldo Correia Filho, Antônio Celso Dantas Antonino, Daniel Duarte, M. Rodrigues
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Abstract

Carbonate rocks are important for the petroleum industry, as they contribute significantly to hydrocarbon reserves, although their analysis is complex due to the high cost of core sampling and their high heterogeneity; for this, synthetic rocks aim to provide relatively homogeneous samples with analogous characteristics to natural rocks. In this research, synthetic carbonate rocks were produced by mixing a fixed ratio between limestone powder, obtained from limestone mining waste, and epoxy resin as a cementing material, using compaction energy for consolidation. The work aimed to produce homogeneous samples with high strength, reproducing the intergranular pore system for future applications in rock–fluid interaction analysis. The characteristics and structure of the samples were investigated through X-ray computed microtomography, petrographic images, petrophysical, chemical and geomechanical tests. Results showed a direct increasing relationship between porosity and permeability and a tendency for mechanical strength (UCS) to decrease with increasing porosity. When compared with the natural carbonate rocks, these presented similarities in their mechanical properties and petrophysical measurements, showing that the methodology can be considered as an alternative for the obtention of a realistic material that can be used for future experiments regarding rock mechanics and rock–fluid interaction for prediction of carbonate rocks’ behavior.
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利用石灰石采矿废料生产合成碳酸盐岩:矿物学、岩石物理学和地质力学特征描述
碳酸盐岩对石油工业非常重要,因为它们对碳氢化合物储量的贡献很大,但由于岩芯取样成本高且异质性强,对它们的分析非常复杂。在这项研究中,合成碳酸盐岩是通过将从石灰石采矿废料中提取的石灰石粉与作为胶结材料的环氧树脂按固定比例混合,并利用压实能进行固结而制成的。这项工作的目的是制作具有高强度的均匀样品,再现晶间孔隙系统,以便将来应用于岩石-流体相互作用分析。通过 X 射线计算机显微层析、岩相图像、岩石物理、化学和地质力学测试,对样品的特征和结构进行了研究。结果表明,孔隙度与渗透率之间存在直接的递增关系,机械强度(UCS)随着孔隙度的增加呈下降趋势。与天然碳酸盐岩相比,这些岩石在机械性能和岩石物理测量方面具有相似性,这表明该方法可被视为获得真实材料的替代方法,可用于未来有关岩石力学和岩石-流体相互作用的实验,以预测碳酸盐岩的行为。
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