Revealing dislocation activity modes during yielding and uniform deformation of low-temperature tempered steel by acoustic emission

Jie Li, Jia-zhi Zhang, Li-yang Zeng, Shuai Wang, Xiang-yu Song, Nai-lu Chen, Xun-wei Zuo, Yong-hua Rong
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Abstract

The distinctive distribution of acoustic emission (AE) characteristic parameters generated during tensile testing of low-temperature tempered AISI 4140 steel was investigated. Two clusters of acoustic emission signals were distinguished using power-law distribution fitting and k-means clustering methods. These clusters were identified as resulting from dislocation motion during yielding and dislocation entanglement during uniform plastic deformation. The conclusion is further confirmed by transmission electron microscopy images at different strains. In particular, the unique "arch-shaped" distribution of the acoustic emission energy during yielding implies a change in unusual dislocation motion modes. The effect of carbide precipitation was qualitatively discussed as not considering the primary cause of the formation of this arch-shaped distribution. The evolution of dislocation motion modes during yielding of low-temperature tempered martensite was elucidated by comparing the significant difference in cumulative energy values during yielding of annealed and low-temperature tempered specimens. Dislocations emit from Frank–Read or grain boundary sources and slip along short free paths, contributing to the initial increase in AE signals energy. Subsequently, the primary source of acoustic emission energy “arch-shaped” peak during yielding was generated by the avalanche behavior of accumulated dislocations, leading to the accelerated dislocation motion.

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利用声发射揭示低温回火钢屈服和均匀变形过程中的位错活动模式
研究了低温回火 AISI 4140 钢拉伸测试过程中产生的声发射(AE)特征参数的独特分布。使用幂律分布拟合和 k-means 聚类方法区分了两个声发射信号群。这些群组被确定为屈服过程中的位错运动和均匀塑性变形过程中的位错缠结所致。不同应变下的透射电子显微镜图像进一步证实了这一结论。特别是,屈服过程中声波发射能量的独特 "拱形 "分布意味着不寻常的位错运动模式发生了变化。对碳化物析出的影响进行了定性讨论,认为它并不是形成这种拱形分布的主要原因。通过比较退火试样和低温回火试样屈服过程中累积能量值的显著差异,阐明了低温回火马氏体屈服过程中位错运动模式的演变。位错从弗兰克读数源或晶界源发出,沿短自由路径滑动,导致 AE 信号能量的初始增加。随后,屈服期间声发射能量 "拱形 "峰的主要来源是累积位错的雪崩行为,导致位错运动加速。
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来源期刊
自引率
16.00%
发文量
161
审稿时长
2.8 months
期刊介绍: Publishes critically reviewed original research of archival significance Covers hydrometallurgy, pyrometallurgy, electrometallurgy, transport phenomena, process control, physical chemistry, solidification, mechanical working, solid state reactions, materials processing, and more Includes welding & joining, surface treatment, mathematical modeling, corrosion, wear and abrasion Journal of Iron and Steel Research International publishes original papers and occasional invited reviews on aspects of research and technology in the process metallurgy and metallic materials. Coverage emphasizes the relationships among the processing, structure and properties of metals, including advanced steel materials, superalloy, intermetallics, metallic functional materials, powder metallurgy, structural titanium alloy, composite steel materials, high entropy alloy, amorphous alloys, metallic nanomaterials, etc..
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