β-Nitroacrylates and Phenols as Key Precursors of Arenofuran-3-carboxylates

Synthesis Pub Date : 2024-07-16 DOI:10.1055/a-2367-1877
Benedetta Bassetti, Matteo Principi, R. Ballini, M. Petrini, A. Palmieri
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Abstract

Herein we report a new practical and efficient preparation of benzofuran and naphthofuran-3-carboxylates starting from β-nitroacrylates and phenols. The reaction is promoted by indium trichloride and leads the target compounds from good to very good yields under microwave irradiations.

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作为阿伦呋喃-3-羧酸盐关键前体的β-硝基丙烯酸酯和酚类化合物
在此,我们报告了一种以 β-硝基丙烯酸酯和苯酚为原料制备苯并呋喃和萘并呋喃-3-羧酸盐的实用高效新方法。该反应在三氯化铟的促进下,在微波辐照下,目标化合物的收率从良好到非常好。
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