Microwave-assisted Synthesis of Cobalt Oxide Nanoparticles with Carica papaya Leaf Extract and their Catalytic Activities

V. Sridhar, Y. Prashanthi, Tentu Nageswara Rao, T. M. Naidu
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Abstract

The Physico-chemical and optical characteristics of cobalt oxide nanoparticles (CoONPs) have attracted interest in their creation over the past few years. In the current study, microwave irradiation was used to induce the production of CoONPs from papaya leaf extract. Papaya leaf extract was prepared by pulverizing and drying the plant's leaves. The extract was then heated to create an aqueous extract, which was purified and saved for analysis. Cobalt nitrate was added to the extract, and a dark brown color was obtained. CoO NPs were used as a catalyst in the reduction of MB and CR, with a mixture of MB solution and NaBH4 in DD water. The catalytic reduction of 4-NP was also tested using CoO NPs. The experimental procedures for characterizing Carica papaya leaf extract CoO NPs include UV-Vis spectra, TEM, and FTIR for analyzing nanomaterial morphology, size, and chemical composition. X-ray Diffraction (XRD) spectroscopy provides information about the crystalline structure, which is crucial for understanding nanomaterial behavior and potential applications in fields like medicine, electronics, and materials science. These methods are critical for understanding nanomaterial behavior and potential applications in various fields.
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用木瓜叶提取物微波辅助合成氧化钴纳米粒子及其催化活性
过去几年来,氧化钴纳米粒子(CoONPs)的物理化学和光学特性引起了人们对其创造的兴趣。在本研究中,使用微波辐照诱导木瓜叶提取物生产 CoONPs。木瓜叶提取物是通过粉碎和干燥木瓜叶而制备的。然后将提取物加热,形成水提取物,并将其纯化和保存以备分析。在提取物中加入硝酸钴,得到深棕色的提取物。在甲基溴溶液和 NaBH4 在 DD水中的混合物中,将 CoO NPs 用作还原甲基溴和 CR 的催化剂。还使用 CoO NPs 测试了 4-NP 的催化还原。木瓜叶提取物 CoO NPs 的表征实验程序包括紫外可见光谱、TEM 和傅立叶变换红外光谱,用于分析纳米材料的形态、尺寸和化学成分。X 射线衍射(XRD)光谱可提供有关晶体结构的信息,这对了解纳米材料的行为以及在医学、电子学和材料科学等领域的潜在应用至关重要。这些方法对于了解纳米材料的行为和在各个领域的潜在应用至关重要。
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