A Surface Topographical Analysis of Lithium Disilicate Ceramics Pretreated With Rose Bengal, Er:YAG Laser, and Ceramic Primer on Bond Integrity, Surface Roughness, and Bond Failure to Composite Resin

IF 0.9 4区 材料科学 Science of Advanced Materials Pub Date : 2024-07-01 DOI:10.1166/sam.2024.4668
Basil Almutairi, A. Al-Qahtani, Tooba Shabbir, Manisha Jagdesh Leemani, Javaid Unar, Neha Manzar, T. Abduljabbar
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Abstract

To evaluate adhesive bond integrity and surface roughness (Ra) of LDS ceramics following various surface modification treatments. Forty LDS ceramic disks were manufactured and allocated into distinct groups according to the pretreatment procedure. Group 1 samples were treated with HF (hydrofluoric acid) and S (silane). Group 2 uses RBe (Rose Bengal photosensitizer) S. Group 3 utilizes SECP (self-etch ceramic primer), while Group 4 employs Er:YAG laser. The Ra, shear bond strength (SBS), and surface topography of the conditioned LDS ceramic were evaluated. The bonding of all LDS ceramics was assessed with a universal testing machine. Debonded samples were analyzed using a stereomicroscope. The Ra and bond integrity values were assessed through the utilization of a two-way ANOVA, followed by Tukey post hoc testing. The samples prepared with HF+S displayed the highest Ra and bond values. However, group 2 (RBe+S) exhibited the least bond strength. There were no notable disparities in the results regarding the strength of the bonds among group 1, group 3 (SECP), and group 4 (Er:YAG laser+S). Er:YAG and SECP show promise as potential substitutes for hydrofluoric acid (HFA) in conditioning LDS ceramics, yielding satisfactory bond scores by positively altering the surface morphology.
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用玫瑰红、Er:YAG 激光和陶瓷底漆预处理的二硅酸锂陶瓷表面形貌分析对复合树脂粘接完整性、表面粗糙度和粘接失败的影响
评估各种表面改性处理后 LDS 陶瓷的粘接完整性和表面粗糙度(Ra)。生产了 40 个 LDS 陶瓷盘,并根据预处理程序分成不同的组。第 1 组样品使用 HF(氢氟酸)和 S(硅烷)处理。第 2 组使用 RBe(玫瑰红光敏剂)S,第 3 组使用 SECP(自刻陶瓷底漆),第 4 组使用 Er:YAG 激光。对经过调理的 LDS 陶瓷的 Ra、剪切粘接强度(SBS)和表面形貌进行了评估。所有 LDS 陶瓷的粘结情况都用万能试验机进行了评估。使用体视显微镜对脱胶样品进行分析。通过双向方差分析评估了 Ra 和粘结完整性值,然后进行了 Tukey 后检验。用 HF+S 制备的样品显示出最高的 Ra 值和结合力值。然而,第 2 组(RBe+S)的粘结强度最低。第 1 组、第 3 组(SECP)和第 4 组(Er:YAG 激光+S)的结合强度没有明显差异。Er:YAG 和 SECP 有望成为氢氟酸 (HFA) 的潜在替代品,用于调节 LDS 陶瓷,通过积极改变表面形态获得令人满意的粘接分数。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Science of Advanced Materials
Science of Advanced Materials NANOSCIENCE & NANOTECHNOLOGY-MATERIALS SCIENCE, MULTIDISCIPLINARY
自引率
11.10%
发文量
98
审稿时长
4.4 months
期刊最新文献
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