Effect of laser process parameters on the pores, surface roughness, and hardness of laser selective melting of dental cobalt-chrome alloys.

Lei Sang, Jiazhen Yan, Ning Li, Chenglai Xin, Qun Wang, Chang Liu
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Abstract

Objectives: To address the quality problems caused by high porosity in the preparation of dental cobalt-chrome alloy prosthetics based on selective laser melting (SLM) technology, we investigated the influence mechanism of different forming process parameters on the microstructure and properties of the materials. Moreover, the range of forming process parameters that can effectively reduce defects was precisely defined.

Methods: The effects of laser power, scanning speed, and scanning distance on the pore properties, surface roughness, and hardness of dental cobalt-chrome alloy were investigated by adjusting the printing parameters in the process of SLM. Through metallographic analysis, image analysis, and molten pool simulation, the pore formation mechanism was revealed, and the relationship between the porosity and energy density of SLM dental cobalt-chrome alloy was elucidated.

Results: When the linear energy density was higher than 0.18 J/mm, the porosity defect easily appeared at the bottom of the molten pool. When the laser energy density was lower than 0.13 J/mm, defects occurred in the gap of the molten pool due to insufficient melting of powder. In particular, when the linear energy density exceeded the threshold of 0.30 J/mm or was below 0.12 J/mm, the porosity increased significantly to more than 1%. In addition, we observed a negative correlation between free surface roughness and energy density and an inverse relationship between macroscopic hardness and porosity.

Conclusions: On the basis of the conditions of raw materials and molding equipment used in this study, the key process parameters of SLM of molding parts with porosity lower than 1% were successfully determined. Specifically, these key parameters included the line energy density, which ranged from 0.13 J/mm to 0.30 J/mm, and the scan spacing should be strictly controlled below 90 μm.

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激光工艺参数对激光选择性熔化牙科钴铬合金的孔隙、表面粗糙度和硬度的影响。
目的:为了解决基于选择性激光熔化(SLM)技术制备牙科钴铬合金修复体时因高孔隙率而导致的质量问题,我们研究了不同成型工艺参数对材料微观结构和性能的影响机制。此外,还精确界定了能有效减少缺陷的成型工艺参数范围:方法:通过调整 SLM 过程中的打印参数,研究了激光功率、扫描速度和扫描距离对牙科钴铬合金孔隙性能、表面粗糙度和硬度的影响。通过金相分析、图像分析和熔池模拟,揭示了孔隙的形成机理,并阐明了 SLM 牙科钴铬合金的孔隙率与能量密度之间的关系:结果:当线性能量密度高于 0.18 J/mm 时,熔池底部容易出现气孔缺陷。当激光能量密度低于 0.13 J/mm 时,由于粉末熔化不充分,熔池间隙中会出现缺陷。特别是当线性能量密度超过 0.30 J/mm 的临界值或低于 0.12 J/mm 时,孔隙率显著增加,超过 1%。此外,我们还观察到自由表面粗糙度与能量密度之间呈负相关,宏观硬度与孔隙率之间呈反比关系:在本研究所用原材料和成型设备条件的基础上,成功确定了气孔率小于 1%的成型零件 SLM 的关键工艺参数。具体而言,这些关键参数包括线能量密度,其范围为 0.13 J/mm 至 0.30 J/mm,扫描间距应严格控制在 90 μm 以下。
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