Effect of artificial aging on optical properties of ultra-translucent zirconia ceramics of different brands.

Luona Chen, Xin Zhang, Zhengyu Tian, Jian Wang
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Abstract

Objectives: This work aimed to evaluate the effect of artificial aging on the translucency and color difference (ΔE) of ultra-translucent zirconia and provide a reference for clinical application.

Methods: The discs of ultra-translucent zirconia from six brands (Wieland, 3M ESPE, Amann Girrbach, Kuraray Noritake, Upcera, and Besmile) were cut and sintered according to each manufacturer's product instructions; the experimental groups were named ZNT, LVP, AG, KAT, UPC, and BSM, respectively. IPS e.max Press was used as the control group (PLT). The specimens (n=6) were prepared with a diameter of 14 mm and a thickness of 1 mm. The specimens were subjected to artificial aging treatment according to the following conditions: in an autoclave at 134 ℃ at 0.2 MPa for 4, 8, and 12 h. According to the CIE1976Lab system, the CIE L*, a*, and b* values of the specimens before and after aging were measured by a co-lorimeter. The translucency parameter (TP) and ΔE were calculated.

Results: The mean TP values of each group before aging inorder were PLT>KAT>AG>ZNT>BSM>UPC>LVP. We found no significant difference in translucency in all experimental groups after aging for 4 and 8 h compared with those before aging. After 12 h of aging, the TP values of the KAT and ZNT groups were not significantly different from those before aging, but the TP values of the AG, BSM, LVP, and UPC groups were significantly lower than those before aging (P<0.05). The TP value of the control group was significantly higher than that of the other experimental groups at different stages (P<0.05). ΔE=3.3 was considered the visible color difference, and ΔE was less than 3.3 in all groups after 4 h of aging. After aging for 8 h, ΔE of the UPC group was slightly higher than 3.3. ΔE of the BSM and UPC groups was greater than 3.3 after 12 h of aging.

Conclusions: The TP and ΔE of different brands of ultra-translucent zirconia may change after various aging times. The translucency of some zirconia showed a decreasing trend and the color difference showed an increasing trend with the aging time.

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人工老化对不同品牌超半透明氧化锆陶瓷光学特性的影响
目的:本研究旨在评估人工老化对超透氧化锆透光度和色差(ΔE)的影响,并为临床应用提供参考:本研究旨在评估人工老化对超透氧化锆透光度和色差(ΔE)的影响,为临床应用提供参考:方法:将六种品牌(Wieland、3M ESPE、Amann Girrbach、Kuraray Noritake、Upcera和Besmile)的超半透明氧化锆盘按照各制造商的产品说明进行切割和烧结,实验组分别命名为ZNT、LVP、AG、KAT、UPC和BSM。IPS e.max Press 用作对照组(PLT)。试样(n=6)直径为 14 毫米,厚度为 1 毫米。试样按照以下条件进行人工老化处理:在 134 ℃、0.2 兆帕的高压锅中分别老化 4、8 和 12 小时。根据 CIE1976Lab 系统,用 co-lorimeter 测量老化前后试样的 CIE L*、a* 和 b* 值。结果:老化前各组的平均 TP 值依次为 PLT>KAT>AG>ZNT>BSM>UPC>LVP。老化 4 和 8 小时后,我们发现所有实验组的透光度与老化前相比无明显差异。老化 12 小时后,KAT 组和 ZNT 组的 TP 值与老化前相比无明显差异,但 AG 组、BSM 组、LVP 组和 UPC 组的 TP 值明显低于老化前(PPConclusions:不同品牌的超半透明氧化锆的 TP 和 ΔE 在不同的老化时间后可能会发生变化。一些氧化锆的半透明度随着老化时间的延长呈下降趋势,而色差则呈上升趋势。
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