Determination of α lamellae orientation in a β-Ti alloy using electron backscatter diffraction.

IF 6.1 3区 材料科学 Q1 Biochemistry, Genetics and Molecular Biology Journal of Applied Crystallography Pub Date : 2024-06-27 eCollection Date: 2024-08-01 DOI:10.1107/S160057672400400X
Petr Harcuba, Jana Šmilauerová, Miloš Janeček, Jan Ilavský, Václav Holý
{"title":"Determination of α lamellae orientation in a β-Ti alloy using electron backscatter diffraction.","authors":"Petr Harcuba, Jana Šmilauerová, Miloš Janeček, Jan Ilavský, Václav Holý","doi":"10.1107/S160057672400400X","DOIUrl":null,"url":null,"abstract":"<p><p>The spatial orientation of α lamellae in a metastable β-Ti matrix of Timetal LCB (Ti-6.8 Mo-4.5 Fe-1.5 Al in wt%) was examined and the orientation of the hexagonal close-packed α lattice in the α lamella was determined. For this purpose, a combination of methods of small-angle X-ray scattering, scanning electron microscopy and electron backscatter diffraction was used. The habit planes of α laths are close to {111}<sub>β</sub>, which corresponds to (1320)<sub>α</sub> in the hexagonal coordinate system of the α phase. The longest α lamella direction lies approximately along one of the 〈110〉<sub>β</sub> directions which are parallel to the specific habit plane. Taking into account the average lattice parameters of the β and α phases in aged conditions in Timetal LCB, it was possible to index all main axes and faces of an α lath not only in the cubic coordinate system of the parent β phase but also in the hexagonal system of the α phase.</p>","PeriodicalId":14950,"journal":{"name":"Journal of Applied Crystallography","volume":"57 Pt 4","pages":"1001-1010"},"PeriodicalIF":6.1000,"publicationDate":"2024-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11299603/pdf/","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Applied Crystallography","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1107/S160057672400400X","RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2024/8/1 0:00:00","PubModel":"eCollection","JCR":"Q1","JCRName":"Biochemistry, Genetics and Molecular Biology","Score":null,"Total":0}
引用次数: 0

Abstract

The spatial orientation of α lamellae in a metastable β-Ti matrix of Timetal LCB (Ti-6.8 Mo-4.5 Fe-1.5 Al in wt%) was examined and the orientation of the hexagonal close-packed α lattice in the α lamella was determined. For this purpose, a combination of methods of small-angle X-ray scattering, scanning electron microscopy and electron backscatter diffraction was used. The habit planes of α laths are close to {111}β, which corresponds to (1320)α in the hexagonal coordinate system of the α phase. The longest α lamella direction lies approximately along one of the 〈110〉β directions which are parallel to the specific habit plane. Taking into account the average lattice parameters of the β and α phases in aged conditions in Timetal LCB, it was possible to index all main axes and faces of an α lath not only in the cubic coordinate system of the parent β phase but also in the hexagonal system of the α phase.

查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
利用电子反向散射衍射法测定β-钛合金中的α层取向。
研究了 Timetal LCB(钛-6.8 钼-4.5 铁-1.5 铝,重量百分比)的可蜕变β-钛基体中的α薄片的空间取向,并确定了α薄片中六方紧密堆积α晶格的取向。为此,结合使用了小角 X 射线散射、扫描电子显微镜和电子反向散射衍射等方法。α薄片的习性平面接近{111}β,相当于α相六方坐标系中的(1320)α。最长的α薄片方向大致沿着与特定习性平面平行的〈110〉β方向之一。考虑到 β 和 α 相在 Timetal LCB 中老化条件下的平均晶格参数,不仅可以在母体 β 相的立方坐标系中,还可以在 α 相的六方坐标系中,对 α 薄片的所有主轴线和面进行索引。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
CiteScore
10.00
自引率
3.30%
发文量
178
审稿时长
4.7 months
期刊介绍: Many research topics in condensed matter research, materials science and the life sciences make use of crystallographic methods to study crystalline and non-crystalline matter with neutrons, X-rays and electrons. Articles published in the Journal of Applied Crystallography focus on these methods and their use in identifying structural and diffusion-controlled phase transformations, structure-property relationships, structural changes of defects, interfaces and surfaces, etc. Developments of instrumentation and crystallographic apparatus, theory and interpretation, numerical analysis and other related subjects are also covered. The journal is the primary place where crystallographic computer program information is published.
期刊最新文献
SUBGROUPS: a computer tool at the Bilbao Crystallographic Server for the study of pseudo-symmetric or distorted structures. Characterization of sub-micrometre-sized voids in fixed human brain tissue using scanning X-ray microdiffraction. Electronic angle focusing for neutron time-of-flight powder diffractometers. Link between b.c.c.-f.c.c. orientation relationship and austenite morphology in CF8M stainless steel. In situ counter-diffusion crystallization and long-term crystal preservation in microfluidic fixed targets for serial crystallography.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1