Mechanical properties of teguline clay pellet mixtures during continuous oedometric compression

IF 5.3 2区 地球科学 Q2 CHEMISTRY, PHYSICAL Applied Clay Science Pub Date : 2024-08-20 DOI:10.1016/j.clay.2024.107535
Peng-Ju Qin , Marsheal Fisonga , Yong-Feng Deng , Yu-Jun Cui , Wei-Min Ye
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Abstract

Clay pellet mixtures are generally compressed to improve their engineering performance. Deepening the comprehension of the mechanical properties of these mixtures in the complete compression process facilitates the benefit to the engineering design and their utilization. In this study, the effects of soil grain size distribution, water content and dry density on the mechanical properties and microstructure of Teguline clay pellet mixtures during a continuous oedometric compression process are explored. Three types of soil pellet mixtures, including mixture A (grain size ≤5 mm), mixture B (≤ 0.4 mm) and mixture C (2–5 mm), were prepared with different water contents of 7%, 8% and 12% respectively. Subsequently, continuous oedometeric compression was undertaken to explore their mechanical behaviours of the soil pellet mixtures. After that, the microstropic structures of the compacted pellet mixtures were investigated using mercury intrusion porosimetry (MIP). The results indicated that mixture A has a minimal initial packing density of pellet mixtures, while mixture C has a maximum one at the initial compression stage. After completion of compression, the compression curves of the pellet mixtures tended to converge uniformity at a semilogarithm coordinate as the vertical stress increased. All of the compression curves presented a concave shape at the plastic compression stage, which is significantly influenced by grain size distribution and water content. In contrast, the elastic compression and rebound behaviours are little affected by the grain size distribution and water content. As far as the microstructure is concerned, compacted samples prepared by mixture A or C presented a unimodal pore structure, while those by mixture B showcased a bimodal pore structure. In comparison with the unimodal pore distribution of the undisturbed stiff clay, the compacted samples displayed a pseudo-unimodal pore distribution because the inter-aggregate pores still existed. A double tangent method was proposed to determine the delimiting pore diameter of the pseudo-unimodal pore distribution curves and found that the delimiting pore diameter decreased with the increase of dry density and water content. Moreover, the inflexion point for the pore diameter of compacted samples prepared by coarse soil was larger than that of fine soil. Combining this work with previous research, it was found that the high compression of coarse soil easily causes the pseudo-unimodal shape, which is also impacted by water content and particle properties. This work could help deepen the understanding of the mechanical characteristics and microstructure of the stiff clay pellet mixtures during continuous oedometric compression.

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茶陵粘土球团混合物在连续 Oedometric 压缩过程中的机械特性
粘土球团混合物通常通过压缩来改善其工程性能。加深对这些混合物在整个压缩过程中的力学性能的理解,有利于工程设计及其利用。在本研究中,我们探讨了土的粒度分布、含水量和干密度对特古林粘土团粒混合物在连续气相压缩过程中的力学性能和微观结构的影响。制备了三种土壤颗粒混合物,包括混合物 A(粒度≤5 毫米)、混合物 B(≤0.4 毫米)和混合物 C(2-5 毫米),其含水量分别为 7%、8% 和 12%。随后,进行了连续气压试验,以探索颗粒土混合物的机械性能。然后,使用汞侵入孔隙模拟法(MIP)研究了压实后颗粒混合物的微观结构。结果表明,混合物 A 的颗粒混合物初始堆积密度最小,而混合物 C 在初始压缩阶段的堆积密度最大。压缩完成后,随着垂直应力的增加,颗粒混合物的压缩曲线在半对数坐标处趋于一致。所有压缩曲线在塑性压缩阶段都呈现凹形,这在很大程度上受到粒度分布和含水量的影响。相比之下,弹性压缩和回弹行为受粒度分布和含水量的影响很小。就微观结构而言,用混合物 A 或 C 制备的压实样品呈现单模态孔隙结构,而用混合物 B 制备的样品则呈现双模态孔隙结构。与未扰动硬质粘土的单峰孔隙分布相比,压实样品显示出假单峰孔隙分布,因为聚集间孔隙仍然存在。提出了一种双正切法来确定伪单峰孔分布曲线的分界孔径,发现分界孔径随着干密度和含水量的增加而减小。此外,粗土制备的压实样品的孔径拐点大于细土。结合前人的研究发现,粗土的高压缩性容易造成假单峰形状,而这种形状也受到含水量和颗粒性质的影响。这项工作有助于加深对硬质粘土颗粒混合物在连续无计量压缩过程中的力学特征和微观结构的理解。
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来源期刊
Applied Clay Science
Applied Clay Science 地学-矿物学
CiteScore
10.30
自引率
10.70%
发文量
289
审稿时长
39 days
期刊介绍: Applied Clay Science aims to be an international journal attracting high quality scientific papers on clays and clay minerals, including research papers, reviews, and technical notes. The journal covers typical subjects of Fundamental and Applied Clay Science such as: • Synthesis and purification • Structural, crystallographic and mineralogical properties of clays and clay minerals • Thermal properties of clays and clay minerals • Physico-chemical properties including i) surface and interface properties; ii) thermodynamic properties; iii) mechanical properties • Interaction with water, with polar and apolar molecules • Colloidal properties and rheology • Adsorption, Intercalation, Ionic exchange • Genesis and deposits of clay minerals • Geology and geochemistry of clays • Modification of clays and clay minerals properties by thermal and physical treatments • Modification by chemical treatments with organic and inorganic molecules(organoclays, pillared clays) • Modification by biological microorganisms. etc...
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