Fundamental Research on Selective Pre-enrichment of Low-Grade Niobium Concentrate from Bayan Obo Mine Via Super Gravity

IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY JOM Pub Date : 2024-08-12 DOI:10.1007/s11837-024-06811-z
Jintao Gao, Rong Yuan, Xi Lan, Huanhuan Xu, Zhancheng Guo
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Abstract

Bayan Obo is the second largest niobium deposit in the world, and has been developed and utilized as iron ore for a long time because of its low niobium content and complex mineral composition. During the high-temperature reduction process, the recovery rate of niobium is low, and most niobium cannot be effectively recovered and utilized. Therefore, a new technology of slag iron separation via super gravity and preconcentration of niobium is proposed in this paper. Firstly, the reduction conditions of niobium concentrate at different temperatures, C/O, and reduction time have been studied to explore the optimal reduction conditions. The results show that the reduction effect was the best at 1200°C, C/O = 1.2 and a reduction time of 60 min. Secondly, under optimal reduction conditions, the super gravity realizes the low-temperature separation of slag and iron. We then studied the effect of C/O, gravity coefficient, and centrifugal time on the super gravity separation of niobium concentrate. The niobium content in slag increased from 4.05% to 15.7%, and the recovery of Nb2O5 reached 94.43%, which greatly improves the niobium grade and is beneficial to the deep processing of niobium concentrate.

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利用超重力对巴彦奥博矿低品位铌精矿进行选择性预富集的基础研究
巴彦奥博是世界第二大铌矿床,由于铌含量低、矿物成分复杂,长期以来一直被作为铁矿石开发利用。在高温还原过程中,铌的回收率较低,大部分铌无法得到有效回收和利用。因此,本文提出了一种通过超重力和预富集铌的渣铁分离新技术。首先,研究了铌精矿在不同温度、C/O 和还原时间下的还原条件,以探索最佳还原条件。结果表明,在 1200°C、C/O = 1.2 和还原时间为 60 分钟时,还原效果最佳。其次,在最佳还原条件下,超重力实现了渣铁的低温分离。然后,我们研究了 C/O、重力系数和离心时间对铌精矿超重力分离的影响。矿渣中的铌含量从 4.05% 提高到 15.7%,Nb2O5 的回收率达到 94.43%,大大提高了铌的品位,有利于铌精矿的深加工。
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来源期刊
JOM
JOM 工程技术-材料科学:综合
CiteScore
4.50
自引率
3.80%
发文量
540
审稿时长
2.8 months
期刊介绍: JOM is a technical journal devoted to exploring the many aspects of materials science and engineering. JOM reports scholarly work that explores the state-of-the-art processing, fabrication, design, and application of metals, ceramics, plastics, composites, and other materials. In pursuing this goal, JOM strives to balance the interests of the laboratory and the marketplace by reporting academic, industrial, and government-sponsored work from around the world.
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