Adsorption performance with field emission scanning electron microscopy of fruit peel induced Silver Nanoparticles in C16H18ClN3S for waste water treatment
{"title":"Adsorption performance with field emission scanning electron microscopy of fruit peel induced Silver Nanoparticles in C16H18ClN3S for waste water treatment","authors":"","doi":"10.1016/j.mex.2024.102951","DOIUrl":null,"url":null,"abstract":"<div><p>There is a growing demand for cost-effective and sustainable technologies for treating wastewater as water consumption increases and conventional technologies become more expensive. Nanoparticles have a great deal of potential for use in the treatment of waste water. Their unique surface area allows them to effectively remove toxic metal ions, pathogenic microorganisms, organic and inorganic solutes from water. This study investigated the potential of orange and banana peels as renewable nano adsorbents for removing dyes and dissolved organic compounds from textile wastewater. Orange and banana peels are an optimal selection due to their favourable chemical characteristics, namely the presence of cellulose, pectic, hemicellulose, and lignin. Their capacity to adsorb diverse anionic and cationic compounds on their surface-active sites is attributed to their unique functional group compositions. Silver nanoparticles are able to adsorb heavy metals due to their exceptionally low electrical and thermal resistance and surface plasmon resonance. The samples were thoroughly characterised using field emission scanning electron microscopy (FESEM), UV–Visible spectrometry, Fourier transform infrared spectroscopy (FTIR) and XRD. The nanoparticles were prepared (10 gm,50 gm,100 gm) and subsequently introduced to the wastewater sample. The optical density values were recorded at various time points. The optical density values demonstrate a decline over the course of the experiment, with a notable decrease observed over time. The results of this study provide valuable insights into the efficacy of these natural adsorbents and their potential for sustainable water purification technologies. For the purpose of this research, high performance instrumentation methods were performed as follows:</p><ul><li><span>•</span><span><p>Field emission scanning electron microscopy for surface morphology studies.</p></span></li><li><span>•</span><span><p>Gas chromatography-mass spectrometry (GC–MS) for analytical technique that combines gas chromatography (GC) and mass spectrometry (MS) to identify unknown substances or contaminants.</p></span></li><li><span>•</span><span><p>Optical density values were measured for different timings of degradation.</p></span></li></ul></div>","PeriodicalId":18446,"journal":{"name":"MethodsX","volume":null,"pages":null},"PeriodicalIF":1.6000,"publicationDate":"2024-09-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S2215016124004023/pdfft?md5=2108bd0864d8b2b8608f1a74705e20a9&pid=1-s2.0-S2215016124004023-main.pdf","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"MethodsX","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2215016124004023","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MULTIDISCIPLINARY SCIENCES","Score":null,"Total":0}
引用次数: 0
Abstract
There is a growing demand for cost-effective and sustainable technologies for treating wastewater as water consumption increases and conventional technologies become more expensive. Nanoparticles have a great deal of potential for use in the treatment of waste water. Their unique surface area allows them to effectively remove toxic metal ions, pathogenic microorganisms, organic and inorganic solutes from water. This study investigated the potential of orange and banana peels as renewable nano adsorbents for removing dyes and dissolved organic compounds from textile wastewater. Orange and banana peels are an optimal selection due to their favourable chemical characteristics, namely the presence of cellulose, pectic, hemicellulose, and lignin. Their capacity to adsorb diverse anionic and cationic compounds on their surface-active sites is attributed to their unique functional group compositions. Silver nanoparticles are able to adsorb heavy metals due to their exceptionally low electrical and thermal resistance and surface plasmon resonance. The samples were thoroughly characterised using field emission scanning electron microscopy (FESEM), UV–Visible spectrometry, Fourier transform infrared spectroscopy (FTIR) and XRD. The nanoparticles were prepared (10 gm,50 gm,100 gm) and subsequently introduced to the wastewater sample. The optical density values were recorded at various time points. The optical density values demonstrate a decline over the course of the experiment, with a notable decrease observed over time. The results of this study provide valuable insights into the efficacy of these natural adsorbents and their potential for sustainable water purification technologies. For the purpose of this research, high performance instrumentation methods were performed as follows:
•
Field emission scanning electron microscopy for surface morphology studies.
•
Gas chromatography-mass spectrometry (GC–MS) for analytical technique that combines gas chromatography (GC) and mass spectrometry (MS) to identify unknown substances or contaminants.
•
Optical density values were measured for different timings of degradation.