Recent advancements in the extraction and analysis of phthalate acid esters in food samples

IF 5.4 2区医学 Q2 MATERIALS SCIENCE, BIOMATERIALS ACS Biomaterials Science & Engineering Pub Date : 2024-09-18 DOI:10.1016/j.foodchem.2024.141262

Qian Yang , Yangqing Wu , Shuaihua Zhang , Hongyu Xie , Dandan Han , Hongyuan Yan

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Abstract

Phthalate acid esters (PAEs) are ubiquitous environmental pollutants present in food samples, necessitating accurate detection for risk assessment and remediation efforts. This review provides an updated overview of the recent progress on the PAEs analysis regarding sample pretreatment techniques and analytical methodologies over the latest decade. Advances in sample preparation include solid-based extraction techniques replacing conventional liquid-liquid extraction, with solid sorbents emerging as promising alternatives due to their minimal solvent consumption and enhanced selectivity. Although techniques like the microextraction methods offer versatility and reduced solvent reliance, there is a need for more efficient and environmentally friendly techniques enabling on-site portable detection. High-resolution mass spectrometry is increasingly utilized for its enhanced sensitivity and reduced contamination risks. However, challenges persist in developing in situ analytical techniques for trace PAEs in complex food samples. Future research should prioritize novel analytical techniques with superior sensitivity and selectivity, addressing current limitations to meet the demand for precise PAEs detection in diverse food matrices.

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提取和分析食品样品中邻苯二甲酸酯的最新进展

邻苯二甲酸酯（PAEs）是食品样本中无处不在的环境污染物，需要进行准确检测，以进行风险评估和补救工作。本综述概述了近十年来 PAEs 分析在样品预处理技术和分析方法方面取得的最新进展。样品预处理方面的进展包括以固体为基础的萃取技术取代了传统的液-液萃取技术，固体吸附剂因其溶剂消耗量极少、选择性更强等优点而成为前景广阔的替代品。尽管微萃取法等技术具有多功能性并减少了对溶剂的依赖，但仍需要更高效、更环保的技术来实现现场便携式检测。高分辨率质谱法因其灵敏度高、污染风险小而得到越来越多的应用。然而，在开发复杂食品样品中痕量 PAEs 的现场分析技术方面仍存在挑战。未来的研究应优先考虑具有卓越灵敏度和选择性的新型分析技术，解决当前的局限性，以满足在各种食品基质中精确检测 PAEs 的需求。

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来源期刊

ACS Biomaterials Science & Engineering Materials Science-Biomaterials

CiteScore

10.30

自引率

3.40%

发文量

413

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