Study on thermal deformation behavior and microstructural evolution of 2 wt. % Al–Ti–C/7075Al composite materials

IF 3.5 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Journal of Materials Science Pub Date : 2024-10-06 DOI:10.1007/s10853-024-10284-5
Ruirui Wu, Ruijun Zhang, Guantao Wang, Fushuai Ding, Bo Gao
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Abstract

Al–Ti–C/7075 aluminum matrix composites (referred to as 7075-ATC) containing uniformly distributed TiC particles and traces of TiAl3 particles were produced by introducing 2 wt. % Al–Ti–C master alloy through stir casting. Isothermal thermal compression behavior at 300 °C–450 °C and 0.001 s−1 to 1 s−1 strain rates was studied in a Gleeble-3800 thermal simulation tester. Peak stress is influenced by deformation temperature and strain rate, reaching its maximum at low temperatures and high strain rates. The activation energy of the final thermal deformation is 150.11 kJ/mol, attributed to particle reinforcement. A sinusoidal hyperbolic Eigen structure equation for composites considering strain compensation is developed to describe the rheological stresses in composites. Dynamic recrystallization at 450 °C and a strain rate of 0.001 s⁻1 enhances composite molding properties. After hot compression, composites exhibit higher activation energy (Q) than cast 7075 and in situ particle-reinforced 7075 due to the obstruction of dislocations by the particles, grain refinement, and pinning effect on the grains. Based on the experimental results, an intrinsic model considering strain compensation was developed to accurately predict the thermal deformation behavior. EBSD results indicated that dynamic softening primarily occurred through dynamic restitution and partial recrystallization. The efficiency of softening peaked at 39% under a strain of 0.6, deformation temperatures between 350 °C and 450 °C, and strain rates ranging from 0.0009 s⁻1 to 0.0111 s⁻1.

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2 wt. % Al-Ti-C/7075Al 复合材料的热变形行为和微结构演变研究
通过搅拌铸造引入 2 wt. % 的 Al-Ti-C 母合金,生产出了含有均匀分布的 TiC 颗粒和微量 TiAl3 颗粒的 Al-Ti-C/7075 铝基复合材料(简称 7075-ATC)。在 Gleeble-3800 热模拟试验机中研究了 300 °C-450 °C 和 0.001 s-1 至 1 s-1 应变速率下的等温热压缩行为。峰值应力受变形温度和应变速率的影响,在低温和高应变速率下达到最大值。最终热变形的活化能为 150.11 kJ/mol,这归因于颗粒强化。考虑到应变补偿,建立了复合材料的正弦双曲特征结构方程来描述复合材料中的流变应力。在 450 °C 和 0.001 s-1 应变速率下的动态再结晶可增强复合材料的成型性能。热压后,由于粒子对位错的阻碍、晶粒细化以及对晶粒的针刺效应,复合材料的活化能(Q)高于铸造 7075 和原位粒子增强 7075。根据实验结果,建立了考虑应变补偿的本征模型,以准确预测热变形行为。EBSD 结果表明,动态软化主要是通过动态回复和部分再结晶发生的。在应变为 0.6、变形温度为 350 °C 至 450 °C 以及应变速率为 0.0009 s-1 至 0.0111 s-1 的条件下,软化效率达到了 39%。
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来源期刊
Journal of Materials Science
Journal of Materials Science 工程技术-材料科学:综合
CiteScore
7.90
自引率
4.40%
发文量
1297
审稿时长
2.4 months
期刊介绍: The Journal of Materials Science publishes reviews, full-length papers, and short Communications recording original research results on, or techniques for studying the relationship between structure, properties, and uses of materials. The subjects are seen from international and interdisciplinary perspectives covering areas including metals, ceramics, glasses, polymers, electrical materials, composite materials, fibers, nanostructured materials, nanocomposites, and biological and biomedical materials. The Journal of Materials Science is now firmly established as the leading source of primary communication for scientists investigating the structure and properties of all engineering materials.
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