Simultaneous measurements of oil- and water-content in crude oil-polluted sands with NMR-deconvolution analysis

IF 2.6 3区 化学 Q2 CHEMISTRY, ANALYTICAL Analytical Methods Pub Date : 2024-10-09 DOI:10.1039/D4AY01052C
Yuxin Wu, Zihan Zhao, Hao Ding, Diansheng Wang and Wei Zhou
{"title":"Simultaneous measurements of oil- and water-content in crude oil-polluted sands with NMR-deconvolution analysis","authors":"Yuxin Wu, Zihan Zhao, Hao Ding, Diansheng Wang and Wei Zhou","doi":"10.1039/D4AY01052C","DOIUrl":null,"url":null,"abstract":"<p >This study introduces a novel deconvolution method for accurately quantifying oil or water signals in the NMR spectra of oil–water–sand mixtures. The algorithm employs a parametric model fitting approach that incorporates prior conditions to set parameters. To validate the approach, the widely overlapping NMR spectra of the complex, synthetic oil–water–sand mixes were separated, and their water and oil contents were determined. The results demonstrated high correlation values and maximum errors of 2.11% and 3.90% for water and oil contents, respectively. The proposed deconvolution method provides an innovative solution for simultaneously measuring the content of each fluid in complex porous media containing multiple fluids by NMR spectroscopy and has the potential to facilitate research in the field.</p>","PeriodicalId":64,"journal":{"name":"Analytical Methods","volume":" 45","pages":" 7823-7830"},"PeriodicalIF":2.6000,"publicationDate":"2024-10-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Analytical Methods","FirstCategoryId":"92","ListUrlMain":"https://pubs.rsc.org/en/content/articlelanding/2024/ay/d4ay01052c","RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, ANALYTICAL","Score":null,"Total":0}
引用次数: 0

Abstract

This study introduces a novel deconvolution method for accurately quantifying oil or water signals in the NMR spectra of oil–water–sand mixtures. The algorithm employs a parametric model fitting approach that incorporates prior conditions to set parameters. To validate the approach, the widely overlapping NMR spectra of the complex, synthetic oil–water–sand mixes were separated, and their water and oil contents were determined. The results demonstrated high correlation values and maximum errors of 2.11% and 3.90% for water and oil contents, respectively. The proposed deconvolution method provides an innovative solution for simultaneously measuring the content of each fluid in complex porous media containing multiple fluids by NMR spectroscopy and has the potential to facilitate research in the field.

Abstract Image

查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
利用核磁共振-解旋分析法同时测量原油污染砂中的油含量和水含量。
本研究介绍了一种新颖的解卷积方法,用于准确量化油-水-沙混合物核磁共振波谱中的油或水信号。该算法采用参数模型拟合方法,结合先验条件设置参数。为了验证该方法,对复杂的合成油-水-沙混合物的广泛重叠核磁共振波谱进行了分离,并确定了它们的水和油含量。结果显示相关值很高,水含量和油含量的最大误差分别为 2.11% 和 3.90%。所提出的解卷积方法为利用核磁共振波谱同时测量含有多种流体的复杂多孔介质中每种流体的含量提供了一种创新的解决方案,有望促进该领域的研究。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
Analytical Methods
Analytical Methods CHEMISTRY, ANALYTICAL-FOOD SCIENCE & TECHNOLOGY
CiteScore
5.10
自引率
3.20%
发文量
569
审稿时长
1.8 months
期刊介绍: Early applied demonstrations of new analytical methods with clear societal impact
期刊最新文献
Ecologically benign S-doped g-C3N4 nano-architectonics for rapid and selective fluorescent detection of the jaundice biomarker bilirubin. Precision traceability of trace psychoactive substances under water quality parameter perturbations in a complex matrix situation. SERS-assisted multivariate data analysis of the spectinomycin-Cu(II) complex released in blood serum from a stimuli-responsive drug carrier: in vitro kinetics modeling and pharmacodynamic analysis. Spectrophotometric determination of the degree of acetylation of cellulose acetate via ferric hydroxamate complexation: method development and validation. Optimised untargeted metabolomics workflow for human urinary extracellular vesicles.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1