Technological and Innovative Features of the Electroconsolidation Method as a Kind of Plasma Sintering for Refractory Compounds

IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Journal of Superhard Materials Pub Date : 2024-10-27 DOI:10.3103/S1063457624050046
E. S. Hevorkian, V. P. Nerubatskyi, V. O. Chyshkala, S. V. Lytovchenko, M. M. Prokopiv, W. Samociuk, V. A. Mechnik
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Abstract

Some physical and technological features of the electroconsolidation process were considered to determine its place among numerous electrodischarge sintering methods. Principal advantages over the other nanopowder compaction methods were noted. The effect of sintering regimes on the formation of a microstructure, the specific features of inhibition under heating in the growth of grains, and the temperature of the graphite press mold and the rate of its heating on the physicomechanical properties of ceramic composites was studied. Some original data on the electroconsolidation process were reposted alongside with the physicochemical properties of nanocomposites synthesized by this method. The probable scheme of electrodischarge processes under high-ampere currents through the graphite press mold is presented.

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作为一种难熔化合物等离子烧结法的电固结法的技术和创新特点
考虑了电固结工艺的一些物理和技术特征,以确定其在众多放电烧结方法中的地位。与其他纳米粉体压制方法相比,电固结工艺的主要优点已被注意到。研究了烧结制度对微观结构形成的影响、加热抑制晶粒生长的具体特点、石墨压模的温度及其加热速度对陶瓷复合材料物理机械性能的影响。在重新发布电固结过程的一些原始数据的同时,还发布了用这种方法合成的纳米复合材料的物理化学性能。介绍了在大安培电流作用下通过石墨压模进行放电过程的可能方案。
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来源期刊
Journal of Superhard Materials
Journal of Superhard Materials MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
1.80
自引率
66.70%
发文量
26
审稿时长
2 months
期刊介绍: Journal of Superhard Materials presents up-to-date results of basic and applied research on production, properties, and applications of superhard materials and related tools. It publishes the results of fundamental research on physicochemical processes of forming and growth of single-crystal, polycrystalline, and dispersed materials, diamond and diamond-like films; developments of methods for spontaneous and controlled synthesis of superhard materials and methods for static, explosive and epitaxial synthesis. The focus of the journal is large single crystals of synthetic diamonds; elite grinding powders and micron powders of synthetic diamonds and cubic boron nitride; polycrystalline and composite superhard materials based on diamond and cubic boron nitride; diamond and carbide tools for highly efficient metal-working, boring, stone-working, coal mining and geological exploration; articles of ceramic; polishing pastes for high-precision optics; precision lathes for diamond turning; technologies of precise machining of metals, glass, and ceramics. The journal covers all fundamental and technological aspects of synthesis, characterization, properties, devices and applications of these materials. The journal welcomes manuscripts from all countries in the English language.
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