Cryogenic fracturing efficacy in granite rocks: Fracture toughness and brazilian test differences after elevated temperatures and liquid nitrogen exposure

Sotirios Nik Longinos, Randy Hazlett
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Abstract

Hot dry rock (HDR) is a significant contingent as a thermal energy source. Due to its low permeability, considerable depth, high temperature (150–650 °C), and high pressure, the stimulation of HDR is challenging. This research work aims to examine the efficacy of cryogenic fracturing on HDR. We performed fracture toughness and indirect tensile stress (Brazilian tests) on granite specimens with three different initial temperatures before exposure to liquid nitrogen (LN2). Fracture toughness tests were implemented on semicircular bend (SCB) specimens containing a pure mode-I fracture, and Brazilian tests were performed with discs. The experimental outcomes show that, overall, both critical load in Brazilian tests and the fracture toughness of LN2-treated specimens of granites both diminished with increasing initial temperature. When the initial temperature exceeded 300 °C (in this instance, 500 °C), the amplitude of thermally induced fractures in granite moderately increased after LN2 treatment, secondary fractures prolonged, and the plastic characteristics increased. Moreover, permeability measurements indicated amelioration with elevated temperatures and subsequent LN2 exposure. SEM analysis showed that an increase in initial temperatures along with LN2 treatment led to further intensified granite microdamage while the quantity and the magnitude of thermal fractures augmented.
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花岗岩的低温压裂效果:高温和液氮暴露后的断裂韧性和巴西试验差异
干热岩(HDR)是一种重要的热能源。由于其渗透率低、埋深大、温度高(150-650 °C)、压力大,对热干岩的开采具有挑战性。这项研究工作旨在考察低温压裂对 HDR 的效果。我们对暴露于液氮(LN2)前具有三种不同初始温度的花岗岩试样进行了断裂韧性和间接拉伸应力(巴西试验)测试。断裂韧性测试是在含有纯 I 型断口的半圆形弯曲(SCB)试样上进行的,巴西试验则是在圆盘上进行的。实验结果表明,总体而言,巴西试验中的临界载荷和经过 LN2 处理的花岗岩试样的断裂韧性都会随着初始温度的升高而降低。当初始温度超过 300 °C(在本例中为 500 °C)时,经 LN2 处理后,花岗岩的热诱导断裂幅度适度增加,二次断裂延长,塑性特征增加。此外,渗透性测量结果表明,随着温度升高和随后的 LN2 暴露,渗透性有所改善。扫描电子显微镜分析表明,随着初始温度的升高和 LN2 处理的进行,花岗岩的微损伤进一步加剧,同时热裂缝的数量和幅度也增加了。
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