Preparation and mechanical behavior of Yb2Si2O7 interphase in SiCf/SiC minicomposites

IF 3.5 3区 材料科学 Q1 MATERIALS SCIENCE, CERAMICS Journal of the American Ceramic Society Pub Date : 2024-09-27 DOI:10.1111/jace.20153
Shuang Mu, Qin Ma, Yu Zhang, Xu Shen, Chunjing Liao, Xiangyu Zhang, Yusheng Ding, Shaoming Dong, Jinshan Yang
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Abstract

In this work, the Yb2Si2O7 interphase was prepared on SiC fibers using the sol–gel method. The influence of sol concentration on the morphology of the interphase was discussed. After heat treatment in argon at 1200°C for 1 h, the Yb2Si2O7 was grown in situ on the fiber surface, forming an interphase layer. Then, SiCf/Yb2Si2O7/SiC minicomposites were prepared by chemical vapor infiltration (CVI). The Yb2Si2O7 interphase exhibited no changes throughout the high-temperature preparation process and maintained stability and compatibility with the fiber and matrix. The tensile strength of SiCf/Yb2Si2O7/SiC minicomposites with Yb2Si2O7 interphase was significantly higher than SiCf/SiC minicomposites without interphase. The crack deflection, interfacial debonding, and fiber pullout were observed in the tensile fracture of the SiCf/Yb2Si2O7/SiC minicomposites.

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SiCf/SiC 微型复合材料中 Yb2Si2O7 相间物的制备与力学行为
本研究采用溶胶-凝胶法在碳化硅纤维上制备了 Yb2Si2O7 相间体。讨论了溶胶浓度对间相形态的影响。在 1200°C 的氩气中热处理 1 小时后,Yb2Si2O7 在纤维表面原位生长,形成相间层。然后,通过化学气相渗透(CVI)制备了 SiCf/Yb2Si2O7/SiC 微型复合材料。在整个高温制备过程中,Yb2Si2O7 相间层没有发生任何变化,并保持了稳定性以及与纤维和基体的相容性。有 Yb2Si2O7 中间相的 SiCf/Yb2Si2O7/SiC 微型复合材料的拉伸强度明显高于无中间相的 SiCf/SiC 微型复合材料。在 SiCf/Yb2Si2O7/SiC 微型复合材料的拉伸断裂中观察到了裂纹偏转、界面脱粘和纤维拉断。
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来源期刊
Journal of the American Ceramic Society
Journal of the American Ceramic Society 工程技术-材料科学:硅酸盐
CiteScore
7.50
自引率
7.70%
发文量
590
审稿时长
2.1 months
期刊介绍: The Journal of the American Ceramic Society contains records of original research that provide insight into or describe the science of ceramic and glass materials and composites based on ceramics and glasses. These papers include reports on discovery, characterization, and analysis of new inorganic, non-metallic materials; synthesis methods; phase relationships; processing approaches; microstructure-property relationships; and functionalities. Of great interest are works that support understanding founded on fundamental principles using experimental, theoretical, or computational methods or combinations of those approaches. All the published papers must be of enduring value and relevant to the science of ceramics and glasses or composites based on those materials. Papers on fundamental ceramic and glass science are welcome including those in the following areas: Enabling materials for grand challenges[...] Materials design, selection, synthesis and processing methods[...] Characterization of compositions, structures, defects, and properties along with new methods [...] Mechanisms, Theory, Modeling, and Simulation[...] JACerS accepts submissions of full-length Articles reporting original research, in-depth Feature Articles, Reviews of the state-of-the-art with compelling analysis, and Rapid Communications which are short papers with sufficient novelty or impact to justify swift publication.
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