Microstructure and mechanical properties of Mg-Gd-Zn-Zr alloy after hot extrusion

IF 6.3 2区 材料科学 Q2 CHEMISTRY, PHYSICAL Journal of Alloys and Compounds Pub Date : 2024-12-02 DOI:10.1016/j.jallcom.2024.177911
Yubo Shen, Qianhao Zang, Sishu Wang, Hongmei Chen, Yuhang Guo, Fengjian Shi, Zhiyuan Zhu
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Abstract

The microstructural evolution and mechanical properties of the Mg-6Gd-1Zn-0.5Zr (wt.%) alloy during heat treatment and composite extrusion were studied in this work. The (Mg, Zn)3Gd phase and a small amount of 14H long-period stacking ordered (LPSO) phase formed in the cast alloy, and more lamellar 14H-LPSO phases formed in the alloy during homogenization treatment. The bimodal grain structure composed of coarse deformed microstructure and fine dynamic recrystallization (DRX) grains formed in the alloy after extrusion. The γ′ phase and β´ phase precipitated after the extrusion process and after the solution and aging treatment, respectively. The kinking of the lamellar 14H-LPSO phase occurred during the extrusion process. DRX grains formed in the alloy during extrusion process through continuous dynamic recrystallization (CDRX), particle stimulated nucleation (PSN), and kinking-assisted DRX. The yield strength, tensile strength and elongation of the extruded alloy were 227 MPa, 320 MPa, and 20.68%, respectively. The strength and elongation of the extruded alloy are enhanced by the strengthening effect from the bimodal structure, kinking of the LPSO phase, and LPSO phase. The tensile properties of the alloy decreased after the solution and aging treatment. The bimodal structure and kinking of the LPSO phase disappeared after the solution and aging treatment.
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Mg-Gd-Zn-Zr合金热挤压后的组织与力学性能
研究了Mg-6Gd-1Zn-0.5Zr (wt.%)合金在热处理和复合挤压过程中的组织演变和力学性能。铸态合金中形成了(Mg, Zn)3Gd相和少量14H长周期有序堆积相(LPSO),均匀化处理后合金中形成了较多的14H-LPSO片层相。挤压后合金中形成由粗大变形组织和细小动态再结晶(DRX)晶粒组成的双峰组织。挤压处理和固溶时效处理后分别析出γ′相和β′相。挤压过程中发生了14H-LPSO层状相的扭结。合金在挤压过程中通过连续动态再结晶(CDRX)、粒子激发成核(PSN)和屈曲辅助DRX形成DRX晶粒。挤压合金的屈服强度为227 MPa,抗拉强度为320 MPa,伸长率为20.68%。双峰组织、LPSO相扭结和LPSO相的强化作用提高了挤压合金的强度和伸长率。固溶时效处理后,合金的拉伸性能下降。固溶时效处理后,LPSO相的双峰结构和扭结消失。
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来源期刊
Journal of Alloys and Compounds
Journal of Alloys and Compounds 工程技术-材料科学:综合
CiteScore
11.10
自引率
14.50%
发文量
5146
审稿时长
67 days
期刊介绍: The Journal of Alloys and Compounds is intended to serve as an international medium for the publication of work on solid materials comprising compounds as well as alloys. Its great strength lies in the diversity of discipline which it encompasses, drawing together results from materials science, solid-state chemistry and physics.
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