Improved mechanical performance and forming accuracy of ZrO2 fixed partial denture based on the digital light processing technology

IF 3.3 2区 医学 Q2 ENGINEERING, BIOMEDICAL Journal of the Mechanical Behavior of Biomedical Materials Pub Date : 2024-11-30 DOI:10.1016/j.jmbbm.2024.106840
Rongfang Zou , Xiaohong Han , Yang Meng , Wenbin Chen , Zhiyun Shi , Yilin Lian , Fangping Wang , Mingzhen Wang , Yang Huang
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Abstract

Fixed partial dentures are the primary treatment for dentition defects. Digital light processing (DLP) 3D printing technology is an advanced technique with significant advantages and potential in the field of dental restoration, particularly in cases requiring high precision and personalization. However, challenges persist in printing fixed partial dentures that meet the strength requirements for clinical applications. In this study, we aimed to optimize printing parameters, including exposure time and layer thickness, to enhance dimensional accuracy, reduce warpage, and improve the surface quality of the samples. Additionally, we focused on the rheological and curing properties of the paste. The optimal combination of printing parameters was found to be 5 s of exposure time and 50 μm layer thickness, achieving superior dimensional accuracy, reduced warpage, and improved surface quality. For a slurry with 40% solid content, the dispersant KOS 110 demonstrated the best shear thinning effect, with an optimal addition of 2%. Notably, the Vickers hardness, flexural strength, and fracture toughness of the ZrO2 fixed partial dentures were 13.52 ± 0.21 GPa, 940 ± 20 MPa, and 6.92 ± 0.25 MPa·m1/2, respectively, which surpasses that of human enamel (4 GPa) and is comparable to CAD/CAM ZrO2 (900–1200 MPa). This study demonstrates that DLP technology can be effectively used to fabricate ZrO2 personalized complex fixed partial dentures with excellent mechanical properties and high precision, offering broad application prospects in stomatology.
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采用数字光加工技术提高了ZrO2固定局部义齿的力学性能和成形精度。
固定部分义齿是治疗牙列缺损的主要方法。数字光处理(DLP) 3D打印技术是一项先进的技术,在牙科修复领域具有显著的优势和潜力,特别是在需要高精度和个性化的情况下。然而,在打印满足临床应用强度要求的固定局部义齿方面仍然存在挑战。在本研究中,我们旨在优化打印参数,包括曝光时间和层厚度,以提高尺寸精度,减少翘曲,改善样品的表面质量。此外,我们重点研究了浆料的流变学和固化性能。结果表明,最佳的打印参数组合为曝光时间为5 s,层厚为50 μm,可获得较好的尺寸精度,减少翘曲,改善表面质量。对于固含量为40%的浆料,分散剂KOS 110的剪切减薄效果最好,最佳添加量为2%。ZrO2固定局部义齿的维氏硬度、抗弯强度和断裂韧性分别为13.52±0.21 GPa、940±20 MPa和6.92±0.25 MPa·m1/2,超过了人牙釉质(4 GPa),与CAD/CAM ZrO2 (900-1200 MPa)相当。本研究表明,DLP技术可有效制备具有优异力学性能和高精度的ZrO2个性化复杂固定局部义齿,在口腔医学中具有广阔的应用前景。
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来源期刊
Journal of the Mechanical Behavior of Biomedical Materials
Journal of the Mechanical Behavior of Biomedical Materials 工程技术-材料科学:生物材料
CiteScore
7.20
自引率
7.70%
发文量
505
审稿时长
46 days
期刊介绍: The Journal of the Mechanical Behavior of Biomedical Materials is concerned with the mechanical deformation, damage and failure under applied forces, of biological material (at the tissue, cellular and molecular levels) and of biomaterials, i.e. those materials which are designed to mimic or replace biological materials. The primary focus of the journal is the synthesis of materials science, biology, and medical and dental science. Reports of fundamental scientific investigations are welcome, as are articles concerned with the practical application of materials in medical devices. Both experimental and theoretical work is of interest; theoretical papers will normally include comparison of predictions with experimental data, though we recognize that this may not always be appropriate. The journal also publishes technical notes concerned with emerging experimental or theoretical techniques, letters to the editor and, by invitation, review articles and papers describing existing techniques for the benefit of an interdisciplinary readership.
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