{"title":"Microwave-Assisted Synthesis and Characterization of Calix[4]resorcinarenes","authors":"P. H. Kanaiya, V. K. Jain","doi":"10.1134/S107042802410018X","DOIUrl":null,"url":null,"abstract":"<p>Microwave irradiation was used to promote the cyclocondensation of certain aldehydes and resorcinol, resulting in a sustainable synthesis of calix[4]resorcinarenes. This environmentally conscious technology possesses numerous attractive characteristics, including high productivity, short reaction time, and straightforward workup protocol. The structures of all calix[4]resorcinarenes were verified using a range of physicochemical techniques, including elemental analysis, FT-IR, <sup>1</sup>H NMR, and mass spectrometry.</p>","PeriodicalId":766,"journal":{"name":"Russian Journal of Organic Chemistry","volume":"60 10","pages":"2014 - 2019"},"PeriodicalIF":0.8000,"publicationDate":"2024-12-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Russian Journal of Organic Chemistry","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1134/S107042802410018X","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, ORGANIC","Score":null,"Total":0}
引用次数: 0
Abstract
Microwave irradiation was used to promote the cyclocondensation of certain aldehydes and resorcinol, resulting in a sustainable synthesis of calix[4]resorcinarenes. This environmentally conscious technology possesses numerous attractive characteristics, including high productivity, short reaction time, and straightforward workup protocol. The structures of all calix[4]resorcinarenes were verified using a range of physicochemical techniques, including elemental analysis, FT-IR, 1H NMR, and mass spectrometry.
期刊介绍：
Russian Journal of Organic Chemistry is an international peer reviewed journal that covers all aspects of modern organic chemistry including organic synthesis, theoretical organic chemistry, structure and mechanism, and the application of organometallic compounds in organic synthesis.
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