{"title":"1-Ethoxy-3-[4-(ethoxycarbonyl)phenyl]-3-hydroxy-1-oxopropan-2-aminium chloride","authors":"Dieter Schollmeyer , Igor Proz , Heiner Detert","doi":"10.1107/S2414314624010320","DOIUrl":null,"url":null,"abstract":"<div><div>The title compound was prepared as a racemate of <em>R</em>,<em>R</em>- and <em>S</em>,<em>S</em>-enantiomers by reduction of the corresponding hydroxyiminoketone. In the crystal, layers are formed <em>via</em> hydrogen bridges of four ammonium groups to chloride ions; these lamellae are connected <em>via</em> interdigitated benzoic ester groups.</div></div><div><div>The title compound, C<sub>14</sub>H<sub>20</sub>NO<sub>5</sub><sup>+</sup>·Cl<sup>−</sup>, was prepared as a racemate of <em>R</em>,<em>R</em>- and <em>S</em>,<em>S</em>-enantiomers by reduction of the corresponding hydroxyiminoketone. In the crystal, layers are formed <em>via</em> hydrogen bridges of four ammonium groups to chloride ions; these lamellae are connected <em>via</em> interdigitated benzoic ester groups.<span><figure><span><img><ol><li><span><span>Download: <span>Download high-res image (223KB)</span></span></span></li><li><span><span>Download: <span>Download full-size image</span></span></span></li></ol></span></figure></span></div></div>","PeriodicalId":94324,"journal":{"name":"IUCrData","volume":"9 10","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2024-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11660177/pdf/","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"IUCrData","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/org/science/article/pii/S241431462400110X","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
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Abstract
The title compound was prepared as a racemate of R,R- and S,S-enantiomers by reduction of the corresponding hydroxyiminoketone. In the crystal, layers are formed via hydrogen bridges of four ammonium groups to chloride ions; these lamellae are connected via interdigitated benzoic ester groups.
The title compound, C14H20NO5+·Cl−, was prepared as a racemate of R,R- and S,S-enantiomers by reduction of the corresponding hydroxyiminoketone. In the crystal, layers are formed via hydrogen bridges of four ammonium groups to chloride ions; these lamellae are connected via interdigitated benzoic ester groups.
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