Sean Power, Louis Free, Ciprian Briciu-Burghina, Chloe Richards, Adrian Delgado, Elena Gomez-Alvarez, Nigel Kent, Fiona Regan
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引用次数: 0
Abstract
Anthropogenic activities have led to increased stress on our marine and other aquatic environments. There is a pressing need to monitor, measure, understand and mitigate causes of these pressures. This paper presents a novel optical head for monitoring and measuring marine based optical phenomena. The development and preliminary testing of the optical head were designed to detect optically active constituents in the marine and coastal environments. Potential applications may include the detection of Harmful Algal Blooms (HAB), which due to their production of toxins have deleterious effects on marine ecosystems, dissolved organic matter (DOM), oil spills, through the measurement of dissolved fluorescent petroleum compounds and turbidity, a key metric in marine and water quality measurements. Preliminary laboratory based results indicate that the optical head is well suited for measuring in-vivo Chlorophyll a (Chl a) fluorescence, turbidity, fluorescent dissolved organic matter (fDOM) and petroleum. For turbidity and in-vivo Chl a, analytical performance was benchmarked against off-the-shelf commercial sensors. The developed optical head demonstrates good analytical performance with certified reference standards and a very good agreement with the reference instrument.
期刊介绍:
Talanta provides a forum for the publication of original research papers, short communications, and critical reviews in all branches of pure and applied analytical chemistry. Papers are evaluated based on established guidelines, including the fundamental nature of the study, scientific novelty, substantial improvement or advantage over existing technology or methods, and demonstrated analytical applicability. Original research papers on fundamental studies, and on novel sensor and instrumentation developments, are encouraged. Novel or improved applications in areas such as clinical and biological chemistry, environmental analysis, geochemistry, materials science and engineering, and analytical platforms for omics development are welcome.
Analytical performance of methods should be determined, including interference and matrix effects, and methods should be validated by comparison with a standard method, or analysis of a certified reference material. Simple spiking recoveries may not be sufficient. The developed method should especially comprise information on selectivity, sensitivity, detection limits, accuracy, and reliability. However, applying official validation or robustness studies to a routine method or technique does not necessarily constitute novelty. Proper statistical treatment of the data should be provided. Relevant literature should be cited, including related publications by the authors, and authors should discuss how their proposed methodology compares with previously reported methods.