Evaluation of Extra-High Translucent Dental Zirconia: Translucency, Crystalline Phase, Mechanical Properties, and Microstructures.

IF 5.2 3区 医学 Q1 ENGINEERING, BIOMEDICAL Journal of Functional Biomaterials Pub Date : 2025-01-03 DOI:10.3390/jfb16010013
Hiroto Nakai, Masanao Inokoshi, Hengyi Liu, Motohiro Uo, Manabu Kanazawa
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Abstract

Highly translucent zirconia (TZ) is frequently used in dentistry. The properties of several highly translucent zirconia materials available in the market require an in-depth understanding. In this study, we assessed the translucency, crystalline phase, mechanical properties, and microstructures of three newly developed highly translucent zirconia materials (Zpex 4. m, 4 mol% yttria-stabilized zirconia: 4YSZ; Zpex Smile.m, 5YSZ; ZR Lucent ULTRA, 6YSZ). The translucency parameter (TP) was analyzed using the CIELAB system. X-ray diffraction was conducted for the crystalline phase analysis, followed by Rietveld refinement. A biaxial flexural strength test using the Weibull analysis was performed to evaluate the mechanical properties. Scanning electron microscopy, grain size distribution, and average grain size were used to analyze the microstructures. The TP content of the ZR Lucent ULTRA was the highest among the samples investigated. The Rietveld analysis revealed that the cubic zirconia phase content of the ZR Lucent ULTRA was the highest. The biaxial flexural strength of the ZR Lucent ULTRA was the lowest (622.9 MPa). The average grain size and proportion of large grains (1.0 µm < x) were the highest in ZR Lucent ULTRA. Therefore, extra-high translucent zirconia has the potential for use in anterior monolithic restorations owing to its esthetics and strength.

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评价超高半透明牙科氧化锆:半透明性、晶相、机械性能和显微结构。
高度半透明的氧化锆(TZ)经常用于牙科。市场上几种高度半透明的氧化锆材料的性能需要深入了解。在这项研究中,我们评估了三种新开发的高半透明氧化锆材料(Zpex 4和Zpex 4)的半透明性、晶相、力学性能和微观结构。m, 4mol %钇稳定氧化锆:4YSZ;Zpex微笑。米,5 ysz;朗讯ULTRA, 6YSZ)。利用CIELAB系统分析了半透明参数(TP)。采用x射线衍射法进行晶相分析,然后进行Rietveld细化。使用威布尔分析进行了双轴弯曲强度测试,以评估机械性能。采用扫描电镜、晶粒尺寸分布和平均晶粒尺寸分析了合金的显微组织。其中,ZR朗讯ULTRA的TP含量最高。Rietveld分析表明,ZR朗讯ULTRA的立方氧化锆相含量最高。ZR朗讯ULTRA的双轴抗折强度最低,为622.9 MPa。ZR朗讯ULTRA的平均晶粒尺寸和大晶粒比例(1.0µm < x)最高。因此,由于其美观和强度,超高半透明氧化锆具有用于前片修复的潜力。
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来源期刊
Journal of Functional Biomaterials
Journal of Functional Biomaterials Engineering-Biomedical Engineering
CiteScore
4.60
自引率
4.20%
发文量
226
审稿时长
11 weeks
期刊介绍: Journal of Functional Biomaterials (JFB, ISSN 2079-4983) is an international and interdisciplinary scientific journal that publishes regular research papers (articles), reviews and short communications about applications of materials for biomedical use. JFB covers subjects from chemistry, pharmacy, biology, physics over to engineering. The journal focuses on the preparation, performance and use of functional biomaterials in biomedical devices and their behaviour in physiological environments. Our aim is to encourage scientists to publish their results in as much detail as possible. Therefore, there is no restriction on the length of the papers. The full experimental details must be provided so that the results can be reproduced. Several topical special issues will be published. Scope: adhesion, adsorption, biocompatibility, biohybrid materials, bio-inert materials, biomaterials, biomedical devices, biomimetic materials, bone repair, cardiovascular devices, ceramics, composite materials, dental implants, dental materials, drug delivery systems, functional biopolymers, glasses, hyper branched polymers, molecularly imprinted polymers (MIPs), nanomedicine, nanoparticles, nanotechnology, natural materials, self-assembly smart materials, stimuli responsive materials, surface modification, tissue devices, tissue engineering, tissue-derived materials, urological devices.
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