Optimizing Si–C reaction bonding for SiC joining: Effects of filler composition, thickness, and surface roughness on joint strength

IF 6.2 2区 材料科学 Q1 MATERIALS SCIENCE, CERAMICS Journal of The European Ceramic Society Pub Date : 2025-07-01 Epub Date: 2025-02-07 DOI:10.1016/j.jeurceramsoc.2025.117269
Sebin Park , Sooyeon Joo , Jong Seob Song , Jung-Hye Eom , Han Nam Cheong , Dang-Hyok Yoon
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Abstract

In this study aims, four key questions regarding the joining of silicon carbide (SiC) via Si–C reaction bonding are explored. These questions address the optimal filler composition for minimizing free Si, the effect of surface roughness on the joint strength, the ideal filler thickness for achieving the maximum joint strength, and the typical defects observed at the joint. To investigate these aspects, SiC was joined using a SiC/C filler tape with varying thicknesses of 10–100 μm, followed by molten Si infiltration at 1500℃ for 1 h under vacuum. Additionally, the surface roughness of the SiC base was adjusted to four levels to evaluate its effect on the joint strength, and common defects were identified. The results indicate that a finely polished SiC base joined with SiC/C = 70/30 wt% tape of ≤ 50 μm thickness achieved a high joint strength of ≥ 250 MPa.
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SiC连接中优化Si-C反应键合:填料成分、厚度和表面粗糙度对连接强度的影响
在本研究中,探讨了通过Si-C反应键连接碳化硅(SiC)的四个关键问题。这些问题涉及到最小化游离硅的最佳填料成分,表面粗糙度对接头强度的影响,达到最大接头强度的理想填料厚度,以及在接头处观察到的典型缺陷。采用厚度为10 ~ 100 μm的SiC/C填充带连接SiC,并在1500℃下真空浸泡1 h。此外,将SiC基体的表面粗糙度调整为4级,以评估其对接头强度的影响,并识别出常见缺陷。结果表明,经过精细抛光的SiC基体与厚度≤ 50 μm的SiC/C = 70/30 wt%带相结合,接头强度达到≥ 250 MPa。
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来源期刊
Journal of The European Ceramic Society
Journal of The European Ceramic Society 工程技术-材料科学:硅酸盐
CiteScore
10.70
自引率
12.30%
发文量
863
审稿时长
35 days
期刊介绍: The Journal of the European Ceramic Society publishes the results of original research and reviews relating to ceramic materials. Papers of either an experimental or theoretical character will be welcomed on a fully international basis. The emphasis is on novel generic science concerning the relationships between processing, microstructure and properties of polycrystalline ceramics consolidated at high temperature. Papers may relate to any of the conventional categories of ceramic: structural, functional, traditional or composite. The central objective is to sustain a high standard of research quality by means of appropriate reviewing procedures.
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