S. Kalecik, E. Güzel, H. E. Gürbüz, F. Kavraz, E. Ağar, M. Yavuz
{"title":"Synthesis, Characterization, FTIR and UV-Vis of a Novel Compound (E)-3-(5-bromo-3-fluoro-2-hydroxybenzilide amino)Benzaldehyde","authors":"S. Kalecik, E. Güzel, H. E. Gürbüz, F. Kavraz, E. Ağar, M. Yavuz","doi":"10.1134/S0022476625010111","DOIUrl":null,"url":null,"abstract":"<p>One of the most studied compound families in the field of crystallography is the Schiff-based compounds. The basis of this research article is a newly synthesized Schiff-base compound. This research aims to investigate the synthesized (<i>E</i>)-3-(5-bromo-3-fluoro-2-hydroxybenzilide amino)benzaldehyde phenol compound using experimental methods. FTIR, UV-Vis and X-ray diffraction methods were used to elucidate the structural properties of the compound synthesized at the end of chemical processes. The structure solution was carried out from the data obtained as a result of X-ray analysis. According to these results, a molecule was formed in the asymmetric cell. The resulting structure has shaped in enol-imine form. The number of molecules in the unit cell was also determined as 4 (<i>Z</i> = 4). According to the results obtained as a result of UV-Vis spectroscopy, the structure revealed that the enol-imine form was dominant. The reasons for this situation were explained.</p>","PeriodicalId":668,"journal":{"name":"Journal of Structural Chemistry","volume":"66 1","pages":"120 - 128"},"PeriodicalIF":1.4000,"publicationDate":"2025-02-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Structural Chemistry","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1134/S0022476625010111","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, INORGANIC & NUCLEAR","Score":null,"Total":0}
引用次数: 0
Abstract
One of the most studied compound families in the field of crystallography is the Schiff-based compounds. The basis of this research article is a newly synthesized Schiff-base compound. This research aims to investigate the synthesized (E)-3-(5-bromo-3-fluoro-2-hydroxybenzilide amino)benzaldehyde phenol compound using experimental methods. FTIR, UV-Vis and X-ray diffraction methods were used to elucidate the structural properties of the compound synthesized at the end of chemical processes. The structure solution was carried out from the data obtained as a result of X-ray analysis. According to these results, a molecule was formed in the asymmetric cell. The resulting structure has shaped in enol-imine form. The number of molecules in the unit cell was also determined as 4 (Z = 4). According to the results obtained as a result of UV-Vis spectroscopy, the structure revealed that the enol-imine form was dominant. The reasons for this situation were explained.
期刊介绍：
Journal is an interdisciplinary publication covering all aspects of structural chemistry, including the theory of molecular structure and chemical bond; the use of physical methods to study the electronic and spatial structure of chemical species; structural features of liquids, solutions, surfaces, supramolecular systems, nano- and solid materials; and the crystal structure of solids.
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