Multifaceted potential of zinc oxide nanoparticles synthesised via thermal decomposition of zinc complexes: characterisation and applications

IF 2.6 4区化学 Q3 CHEMISTRY, PHYSICAL Ionics Pub Date : 2025-01-26 DOI:10.1007/s11581-025-06094-7

V. Preethi, S. Anila Raj, V. G. Viju Kumar, V. G. Vidya

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Abstract

Zinc oxide nanoparticles exhibit distinctive optical, biological, electrical, and catalytic properties that render them extremely promising for an extensive array of applications. For this study, zinc complexes were thermally broken down to synthesis zinc oxide nanoparticles. Complexes were prepared by condensation reaction of N, N′′′Z)-N′,N′′′-(1,2-diphenylethane-1,2-diylidene)di(nicotinohydrazide (BNH) and various zinc salts. Fourier transform infrared spectroscopy, UV–visible, mass spectra, and thermogravimetric analysis were used to characterise zinc complexes. Several analytical techniques were used to characterise the nanoparticles, including X-ray diffraction analysis and electron microscopy including scanning and transmission techniques. Results showed that crystalline zinc oxide nanoparticles with distinct morphologies and nanoscale dimensions were formed. Methylene blue and methyl orange were used to test the potential of zinc oxide nanoparticles as a photocatalyst, and the results were promising. In vitro antidiabetic, in vitro antioxidant, sun protection factor, and in vitro scratch wound healing experiments demonstrated the advantages of zinc oxide nanoparticles.

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通过锌配合物热分解合成氧化锌纳米颗粒的多方面潜力：表征和应用

氧化锌纳米颗粒表现出独特的光学、生物、电学和催化性能，使它们具有广泛的应用前景。在这项研究中，锌配合物被热分解合成氧化锌纳米颗粒。以N， N ' ' Z)-N ',N ' -（1,2-二苯乙烷-1,2-二乙基）二烟肼（BNH）与各种锌盐缩合反应制备配合物。傅里叶变换红外光谱、紫外可见光谱、质谱和热重分析对锌配合物进行了表征。使用了几种分析技术来表征纳米颗粒，包括x射线衍射分析和电子显微镜，包括扫描和透射技术。结果表明，制备的氧化锌纳米颗粒具有不同的形貌和纳米尺度。用亚甲基蓝和甲基橙测试了氧化锌纳米颗粒作为光催化剂的潜力，结果很有希望。体外抗糖尿病、体外抗氧化、防晒因子及体外抓伤愈合实验证明了氧化锌纳米颗粒的优势。图形抽象

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来源期刊

Ionics 化学-电化学

CiteScore

5.30

自引率

7.10%

发文量

427

审稿时长

2.2 months

期刊介绍： Ionics is publishing original results in the fields of science and technology of ionic motion. This includes theoretical, experimental and practical work on electrolytes, electrode, ionic/electronic interfaces, ionic transport aspects of corrosion, galvanic cells, e.g. for thermodynamic and kinetic studies, batteries, fuel cells, sensors and electrochromics. Fast solid ionic conductors are presently providing new opportunities in view of several advantages, in addition to conventional liquid electrolytes.