Synthesis of Fe3O4 Encapsulated with Lemon Yellow for Application in Magnetic Particle Inspection

IF 2.4 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Journal of Nondestructive Evaluation Pub Date : 2025-03-10 DOI:10.1007/s10921-025-01175-z
Zhiqi Liang, Zhili Zhang, Decai Li
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Abstract

Magnetic particle inspection, a widely used nondestructive testing method, is employed to inspect surface defects in ferromagnetic materials due to its ease of operation, low cost, and high efficiency. In this study, Fe3O4 hollow nanospheres were synthesized by a solvothermal method. Lemon yellow (LY) pigments were successfully encapsulated on the surface of these magnetic nanospheres using E51 epoxy resin. The synthesized Fe3O4/E51/LY composite material was characterized in terms of its microscopic morphology, physical phase, and structural properties. The adsorption mechanism of the fluorescent materials on the particle surface was analyzed. Additionally, the photoluminescence and magnetic properties of the composite were tested and evaluated. A magnetic particle inspection test bench was then established to detect defects in the workpiece. The composite exhibited a saturation magnetization of 53.22 emu/g and emitted yellow-green fluorescence at 525 nm under ultraviolet light. The surface defects of the workpiece were accurately detected using magnetic fluorescent particles.

Graphical Abstract

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柠檬黄包封Fe3O4的合成及其在磁粉检测中的应用
磁粉探伤是一种应用广泛的无损检测方法,具有操作简单、成本低、效率高等优点,可用于铁磁性材料表面缺陷的检测。本研究采用溶剂热法制备了Fe3O4空心纳米球。用E51环氧树脂成功地将柠檬黄(LY)颜料包封在磁性纳米球表面。对合成的Fe3O4/E51/LY复合材料进行了微观形貌、物相和结构性能表征。分析了荧光材料在颗粒表面的吸附机理。此外,对复合材料的光致发光性能和磁性能进行了测试和评价。建立了磁粉检测试验台,用于检测工件缺陷。复合材料的饱和磁化强度为53.22 emu/g,在紫外光下发出525 nm的黄绿色荧光。利用磁性荧光颗粒对工件表面缺陷进行了精确检测。图形抽象
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文献相关原料
公司名称
产品信息
麦克林
sodium dodecylbenzene sulfonate
麦克林
lemon yellow
麦克林
E51 epoxy resin
麦克林
ethylene glycol
麦克林
sodium acetate anhydrous
麦克林
Ferric chloride hexahydrate
来源期刊
Journal of Nondestructive Evaluation
Journal of Nondestructive Evaluation 工程技术-材料科学:表征与测试
CiteScore
4.90
自引率
7.10%
发文量
67
审稿时长
9 months
期刊介绍: Journal of Nondestructive Evaluation provides a forum for the broad range of scientific and engineering activities involved in developing a quantitative nondestructive evaluation (NDE) capability. This interdisciplinary journal publishes papers on the development of new equipment, analyses, and approaches to nondestructive measurements.
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