An investigation of Y-TZP surface characteristics and adhesive properties following treatment with Tri-biochemical Silica Coating, Femtosecond Laser, and Nano-hydroxyapatite: A scanning electron microscopy evaluation.

IF 1.2 4区 医学 Q2 MEDICINE, GENERAL & INTERNAL Pakistan Journal of Medical Sciences Pub Date : 2025-03-01 DOI:10.12669/pjms.41.3.11302
Fahad Alkhudhairy, Nourah N Shono
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Abstract

Objectives: To examine how advanced surface pretreatment techniques - Tribochemical silica coating (TBC), Femtosecond laser (FS), and Nano-hydroxyapatite (HA) coating - affect the surface roughness (Ra) and shear bond strength (SBS) between resin luting cement and Yttria-stabilized tetragonal zirconia polycrystals (Y-TZP).

Methods: The lab-based comparative study was approved by the ethical committee of King Saud University under IRB number F98-971X9 and was completed in three months (June to September, 2024). Eighty-four YTZP zirconia discs were created and sorted into four groups based on different conditioning agents: Group-I (APA) as the control, Group-II (TBC), Group-III (FS laser), and Group-IV (Nano-HA coating). Ra was measured on five discs from each group using a profilometer, while surface topography was examined through SEM analysis. Ten specimens per group were bonded with luting cement, followed by SBS testing and fracture mode analysis using a universal testing machine and stereomicroscope, respectively. One-way ANOVA with post hoc Tukey tests (p<0.05) was used for statistical analysis of Ra and SBS means across the groups.

Results: Group-IV (Nano-HA coating) exhibited the highest Ra and SBS values. Conversely, Group II (TBC) displayed the lowest Ra and weakest bond strength.

Conclusion: Nano-HA coating and FS laser can be employed as viable alternatives to APA without compromising the physical and mechanical properties of zirconia ceramic.

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三生化二氧化硅涂层、飞秒激光和纳米羟基磷灰石处理后的 Y-TZP 表面特征和粘合性能研究:扫描电子显微镜评估。
目的:研究先进的表面预处理技术-摩擦化学二氧化硅涂层(TBC),飞秒激光(FS)和纳米羟基磷灰石(HA)涂层-如何影响树脂胶凝水泥和钇稳定的四方氧化锆多晶(Y-TZP)之间的表面粗糙度(Ra)和剪切结合强度(SBS)。方法:本实验室比较研究经沙特国王大学伦理委员会批准,IRB号F98-971X9,于2024年6月至9月3个月内完成。制备了84个YTZP氧化锆圆片,并根据不同的调理剂将其分为4组:ⅰ组(APA)作为对照,ⅱ组(TBC),ⅲ组(FS激光)和ⅳ组(纳米ha涂层)。使用轮廓仪在每组的五个圆盘上测量Ra,同时通过扫描电镜分析检查表面形貌。每组10个试件用芦丁水泥粘结,分别用万能试验机和体视显微镜进行SBS测试和断裂模式分析。单因素方差分析与事后Tukey检验(结果:组iv(纳米ha涂层)显示出最高的Ra和SBS值。相反,组II (TBC)的Ra最低,键强度最弱。结论:在不影响氧化锆陶瓷物理力学性能的前提下,纳米羟基磷灰石涂层和FS激光可作为APA的可行替代品。
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来源期刊
Pakistan Journal of Medical Sciences
Pakistan Journal of Medical Sciences 医学-医学:内科
CiteScore
4.10
自引率
9.10%
发文量
363
审稿时长
3-6 weeks
期刊介绍: It is a peer reviewed medical journal published regularly since 1984. It was previously known as quarterly "SPECIALIST" till December 31st 1999. It publishes original research articles, review articles, current practices, short communications & case reports. It attracts manuscripts not only from within Pakistan but also from over fifty countries from abroad. Copies of PJMS are sent to all the import medical libraries all over Pakistan and overseas particularly in South East Asia and Asia Pacific besides WHO EMRO Region countries. Eminent members of the medical profession at home and abroad regularly contribute their write-ups, manuscripts in our publications. We pursue an independent editorial policy, which allows an opportunity to the healthcare professionals to express their views without any fear or favour. That is why many opinion makers among the medical and pharmaceutical profession use this publication to communicate their viewpoint.
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