Microwave Synthesis of Ag@MoS2 in NADES medium for the Dispersive Micro Solid Phase Extraction of Atrazine in environmental samples

IF 3 4区环境科学与生态学 Q2 ENVIRONMENTAL SCIENCES Water, Air, & Soil Pollution Pub Date : 2025-04-16 DOI:10.1007/s11270-025-07991-3

Furkan Uzcan, Mustafa Soylak

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Abstract

A simple-to-operate, environmentally friendly method has been developed for novel Ag sphere synthesis in NADES media to achieve spherical form and for green synthesis that was modified with MoS₂ nanoparticles. Ag@MoS₂ was designed as an adsorbent for a rapid and economical dispersive micro solid phase extraction approach at trace levels. The Analytical parameters pH (5.0), sorbent mass (10 mg), extraction time (2.5 min), eluent volume (5 mL), eluent type (acetonitrile), and sample volume (10 mL) were optimized. The detection limit was found to be 0.6 μg L^–1 and the technique’s linearity ranged from 2.1 to 250 μg L^–1. The suggested approach has several benefits, including selectivity, precision, and rapidity. It is used practically to identify ATZ in lake water, fish farming water, tap water, allspice and rosehip. The ATZ recovery was sufficient, averaging between 91 and 107%. The method had an overall score of 0.57 on the AGREE scale.

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NADES介质中Ag@MoS2的微波合成用于分散微固相萃取环境样品中的阿特拉津

一种简单、环保的新型银球合成方法在NADES介质中实现球形，并使用二硫化钼纳米颗粒修饰绿色合成。Ag@MoS2被设计为一种快速和经济的分散微固相萃取方法。优化分析参数pH（5.0）、吸附剂质量（10 mg）、萃取时间（2.5 min）、洗脱液体积（5 mL）、洗脱液类型（乙腈）、进样量（10 mL）。检测限为0.6 μg L-1，线性范围为2.1 ~ 250 μg L-1。所建议的方法有几个优点，包括选择性、精确性和快速性。实际应用于湖水、养鱼用水、自来水、多香果和玫瑰果中的ATZ的鉴定。ATZ回收率足够，平均在91 ~ 107%之间。该方法在AGREE量表上的总分为0.57。

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来源期刊

Water, Air, & Soil Pollution 环境科学-环境科学

CiteScore

4.50

自引率

6.90%

发文量

448

审稿时长

2.6 months

期刊介绍： Water, Air, & Soil Pollution is an international, interdisciplinary journal on all aspects of pollution and solutions to pollution in the biosphere. This includes chemical, physical and biological processes affecting flora, fauna, water, air and soil in relation to environmental pollution. Because of its scope, the subject areas are diverse and include all aspects of pollution sources, transport, deposition, accumulation, acid precipitation, atmospheric pollution, metals, aquatic pollution including marine pollution and ground water, waste water, pesticides, soil pollution, sewage, sediment pollution, forestry pollution, effects of pollutants on humans, vegetation, fish, aquatic species, micro-organisms, and animals, environmental and molecular toxicology applied to pollution research, biosensors, global and climate change, ecological implications of pollution and pollution models. Water, Air, & Soil Pollution also publishes manuscripts on novel methods used in the study of environmental pollutants, environmental toxicology, environmental biology, novel environmental engineering related to pollution, biodiversity as influenced by pollution, novel environmental biotechnology as applied to pollution (e.g. bioremediation), environmental modelling and biorestoration of polluted environments. Articles should not be submitted that are of local interest only and do not advance international knowledge in environmental pollution and solutions to pollution. Articles that simply replicate known knowledge or techniques while researching a local pollution problem will normally be rejected without review. Submitted articles must have up-to-date references, employ the correct experimental replication and statistical analysis, where needed and contain a significant contribution to new knowledge. The publishing and editorial team sincerely appreciate your cooperation. Water, Air, & Soil Pollution publishes research papers; review articles; mini-reviews; and book reviews.