Technical parameters of plastics (Mercox CL-2B and various methylmethacrylates) used in scanning electron microscopy of vascular corrosion casts.

Scanning electron microscopy Pub Date : 1986-01-01
T Weiger, A Lametschwandtner, P Stockmayer
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Abstract

The most frequently used resins for vascular corrosion casting Mercox Cl-2B, Mercox Cl-2B diluted with methylmethacrylate (MMA) monomer and various self prepared MMA and hydroxypropyl-methacrylate mixtures were tested with regard to their thermostability, shrinkage, viscosity and replication quality. It was found that tempering of the plastics improves their thermostability with the exception of Mercox Cl-2B and that shrinkage depends on the amount of monomers a resin contains. In detail; Mercox Cl-2B has the lowest shrinkage (8.018%) whereas a hydroxypropyl-methacrylate mixture possessed the highest (20.408%). But, on the other hand, viscosity decreases with the quantity of monomers. All resins tested were able to replicate structures of 260 nm height but the resins' quality of replication was found to be limited by the effects of shrinkage. Finally, a method to estimate the blood volume of organs and tissues with the help of vascular corrosion casts is given.

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用于血管腐蚀铸件扫描电镜的塑料(Mercox CL-2B和各种甲基丙烯酸甲酯)技术参数。
对维管腐蚀铸造最常用的树脂Mercox Cl-2B、用甲基丙烯酸甲酯(MMA)单体稀释的Mercox Cl-2B和各种自制的MMA和甲基丙烯酸羟丙酯混合物的热稳定性、收缩性、粘度和复制性进行了测试。研究发现,除Mercox Cl-2B外,回火可改善塑料的热稳定性,收缩率取决于树脂中单体的含量。详细地;Mercox Cl-2B的收缩率最低(8.018%),羟丙基-甲基丙烯酸酯混合物的收缩率最高(20.408%)。但是,另一方面,粘度随单体数量的增加而降低。所有测试的树脂都能够复制260纳米高度的结构,但发现树脂的复制质量受到收缩的影响。最后,给出了一种利用血管腐蚀模型估计器官和组织血容量的方法。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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