{"title":"A symmetrical vacuum thermoblance for corrosive atmospheres.","authors":"E Pedersen","doi":"10.1088/0022-3735/1/10/310","DOIUrl":null,"url":null,"abstract":"A vacuum thermobalance with symmetrical hang-down and furnace system for samples between 0·1 and 500 mg is described. Flow of nearly every corrosive gas at any constant pressure in the range 0·1 torr to 1 atm can be applied. Zero drift is below 1 μg from 20 to 900°C. As examples of the application are mentioned the reactions in hydrogen chloride atmosphere of tris(ethylendiamine)-and tris(trimethylendiamine) chromium(III) chloride under formation of cis- and trans-dichloro complexes, respectively.","PeriodicalId":16983,"journal":{"name":"Journal of Scientific Instruments","volume":"1 10","pages":"1013-5"},"PeriodicalIF":0.0000,"publicationDate":"1968-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1088/0022-3735/1/10/310","citationCount":"4","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Scientific Instruments","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1088/0022-3735/1/10/310","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 4
Abstract
A vacuum thermobalance with symmetrical hang-down and furnace system for samples between 0·1 and 500 mg is described. Flow of nearly every corrosive gas at any constant pressure in the range 0·1 torr to 1 atm can be applied. Zero drift is below 1 μg from 20 to 900°C. As examples of the application are mentioned the reactions in hydrogen chloride atmosphere of tris(ethylendiamine)-and tris(trimethylendiamine) chromium(III) chloride under formation of cis- and trans-dichloro complexes, respectively.
京公网安备 11010802042870号
京ICP备2023020795号-1
分享
求助内容：
应助结果提醒方式：
扫码关注我们
