{"title":"Electron probe microanalysis of metal oxides.","authors":"C A Friskeny, C W Haworth","doi":"10.1088/0022-3735/1/7/313","DOIUrl":null,"url":null,"abstract":"An experimental procedure for the analysis of nonconducting specimens by using metal standards is described. The specimens are coated with about 100 A of copper by vacuum evaporation to prevent electrostatic charging and to reduce heating effects. It is found that specimens should be preferably dry polished and analysed under fixed time conditions. Application to the analysis of some slags is described and it is found that the use of oxide substandards is not entirely satisfactory.","PeriodicalId":16983,"journal":{"name":"Journal of Scientific Instruments","volume":"1 7","pages":"753-6"},"PeriodicalIF":0.0000,"publicationDate":"1968-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1088/0022-3735/1/7/313","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Scientific Instruments","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1088/0022-3735/1/7/313","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1
Abstract
An experimental procedure for the analysis of nonconducting specimens by using metal standards is described. The specimens are coated with about 100 A of copper by vacuum evaporation to prevent electrostatic charging and to reduce heating effects. It is found that specimens should be preferably dry polished and analysed under fixed time conditions. Application to the analysis of some slags is described and it is found that the use of oxide substandards is not entirely satisfactory.
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