Multiple coatings can improve the bond durability of one-step self-etching adhesive to primary dentin.

Lin Ma, Jian-feng Zhou, Quan Jing, Ji-zhi Zhao, Kuo Wan
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Abstract

Objective: To investigate whether multiple coatings can improve the bond durability of one-step self-etching adhesive to primary dentin.

Methods: Twelve caries-free human primary molars were randomly divided into 2 groups. In group 1, each tooth was hemisected into 2 halves. One half was assigned to the control subgroup 1, which was bonded with a commercially available one-step self-etching adhesive according to the manufacturer's instructions; the other half was assigned to experimental subgroup 1, in which the adhesive was applied three times before light curing. In group 2, one split half tooth was bonded with a commercially available one-step self-etching adhesive according to the manufacturer's instructions; for the other half, three layers of adhesive were applied with each successive layer of light curing. Specimens were stored in 0.9% NaCl containing 0.02% sodium azide at 37℃ for 18 months and then were subjected to microtensile bond strength test and the fracture mode analysis.

Results: When the adhesive was applied three times before light curing, the bond strength of the experimental subgroup 1 was significantly higher than that of the control subgroup 1 (47.46∓13.91 vs. 38.12∓11.21 MPa, P<0.05). When using the technique of applying multiple layers of adhesive with each successive layer of light curing, no difference was observed in bond strength between the control subgroup and the experimental subgroup (39.40±8.87 vs. 40.87±9.33 MPa, P>0.05).

Conclusion: Multiple coatings can improve the bond durability of one-step self-etching adhesive to primary dentin when using the technique of light-curing after applying 3 layers of adhesive.

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复合涂层可提高一步自蚀刻胶与初级牙本质的粘接耐久性。
目的:探讨复合涂层能否提高一步自蚀刻胶与初级牙本质的粘接耐久性。方法:12颗无龋人乳牙随机分为2组。第1组,每颗牙半切成2半。其中一半被分配到对照亚组1,根据制造商的说明,用市售的一步自蚀刻粘合剂粘合;另一半作为实验亚组1,在光固化前涂三次胶粘剂。在第二组中,根据制造商的说明,用市售的一步自蚀刻粘合剂粘合一颗裂开的半齿;对于另一半,在每一层连续的光固化上涂上三层粘合剂。将试样在含0.02%叠氮化钠的0.9% NaCl中37℃保存18个月,进行微拉伸粘结强度测试和断裂模式分析。结果:光固化前涂布3次,实验亚组1的黏结强度显著高于对照亚组1 (47.46 / 13.91 / 38.12 / 11.21 MPa, P0.05)。结论:采用三层光固化技术,多层涂层可提高一步自蚀刻胶与初级牙本质的粘接耐久性。
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