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New way of direct nitrogen atom phenylation in quinoline derivatives.

ISRN Organic Chemistry Pub Date : 2012-07-03 eCollection Date: 2012-01-01 DOI:10.5402/2012/526867

Nadezhda E Shchepina Viktor V Avrorin Gennady A Badun Scott B Lewis Sergey N Shurov

引用次数: 5

Abstract

Comparison of ion-molecular reactions of free-phenyl cations generated by tritium β -decay with 2-methyl- and 2-phenylquinolines has been investigated. The reaction of direct nitrogen atom phenylation with the help of nucleogenic phenyl cations has been fulfilled for the first time and a new one-step synthesis of tritium-labeled N-phenyl-2-phenylquinolinium salt-lipophilic radioactive biological marker has been elaborated.

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喹啉衍生物中氮原子直接苯基化的新方法。

研究了β -氚衰变生成的游离苯基阳离子与2-甲基和2-苯基喹啉的离子分子反应。首次实现了氮原子直接苯基化反应，制备了一种新的一步法合成了氚标记的n -苯基-2-苯喹啉盐亲脂性放射性生物标志物。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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Second Supplements to the 2nd Edition of Rodd's Chemistry of Carbon Compounds. Volume IV. Heterocyclic compounds. Part F. Six-Membered Heterocyclic Compounds with a Single Hetero-Atom in the Ring: Pyridine, Quinoline, Isoquinoline and Their Derivatives. Part G. Six-Membered Heterocyclic Compounds with (a) Single Nitrogen Atom in the Ring (cont'd): Polycyclic Fused Ring Compounds, (b) an Atom of Phosphorous, Arsenic, Antimony or Bismuth. Alkaloids with a Six-Membered Heterocyclic Ring (Chapters 28−33 in this Volume) Edited by M. Sainsbury (University of Bath, Bath England). Elsevier Science BV, Amsterdam. 1998. xx + 620 pp. 15 × 22.5 cm. $379.50. ISBN 0-444-82943-1.

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Second Supplements to the 2nd Edition of Rodd's Chemistry of Carbon Compounds. Vol. IV. Heterocyclic Compounds. Part F. Six-membered Heterocyclic Compounds with a Single Hetero-Atom in the Ring: Pyridine, Quinoline, Isoquinoline and Their Derivatives. Part G. Six-membered Heterocyclic Compounds with (a) a Single Hetero-Atom in the Ring (contd): Polycyclic Fused Ring Compounds, (b) an Atom of Phosphorus, Arsenic, Antimony or Bismuth. Alkaloids with a Six-membered Heterocyclic Ring. Part H. Six-membered Fused-Ring Heterocyclic Compounds with a Single Nitrogen Atom in the Ring (contd): Monocyclic Ring Compounds with Two Hetero-Atoms in the Ring from Group VI B, or One Each from Groups V and VI B. Alkaloids (contd) Edited by M. Sainsbury. Elsevier: New York. 1998. Parts F/G: 650 pp; $402.50; ISBN 0-444-82979-2. Parts G/H: 620 pp; $379.50; ISBN 0-444-82943-1.

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ISRN Organic Chemistry

ISRN Organic Chemistry

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