Influence of niobium pentoxide addition on the properties of glass ionomer cements.

Acta Biomaterialia Odontologica Scandinavica Pub Date : 2016-10-05 eCollection Date: 2016-12-01 DOI:10.1080/23337931.2016.1239182
Isadora Martini Garcia, Vicente Castelo Branco Leitune, Gabriela De Souza Balbinot, Susana Maria Werner Samuel, Fabrício Mezzomo Collares
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引用次数: 20

Abstract

Objective: To determine the influence of niobium pentoxide (Nb2O5) addition on the physical and chemical properties of glass ionomer cements (GICs). Materials and methods: Five, 10 or 20 wt.% of Nb2O5 were incorporated into commercial GICs (Maxxion R, Vitro Molar, Vitro Fil R) and one group of each GIC remained without Nb2O5 (control groups). The GICs were evaluated by Knoop hardness, compressive strength, acid erosion, particle size and radiopacity. Data were analyzed by two-way ANOVA followed by Tukey's test. Results: The addition of 10% and 20% reduced the microhardness of two GICs (p < .05). Compressive strength showed no difference among groups (p > .05). Nb2O5 did not influence Maxxion R and Vitro Fil R regarding the acid erosion test (p > .05). Vitro Molar increased its acid erosion with 10% of Nb2O5 (p < .05). Maxxion R presented 15.78 μm, while Vitro Molar and Vitro Fil R showed 5.14 μm and 6.18 μm, respectively. As the Nb2O5 concentration increased, the radiopacity increased for all groups. Vitro Molar and Vitro Fil R did not present significant difference to at least 1 mm aluminum (p > .05). Conclusion: The addition of 5 wt.% Nb2O5 did not affect the tested physical and chemical properties of the GICs and improved the radiopacity of one of the cements. These materials are therefore suitable for further testing of biomimetic remineralization properties.

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掺加五氧化二铌对玻璃离子水合物性能的影响。
目的:研究五氧化二铌(Nb2O5)对玻璃离子水结剂(gic)理化性能的影响。材料和方法:将5%,10%或20%的Nb2O5加入到商业GIC (Maxxion R,试管磨牙,试管Fil R)中,每种GIC均有一组不含Nb2O5(对照组)。通过努氏硬度、抗压强度、酸侵蚀、粒径和透光度等指标对GICs进行评价。数据分析采用双因素方差分析,然后进行Tukey检验。结果:添加10%和20%降低了两种GICs的显微硬度(p < 0.05)。各组抗压强度差异无统计学意义(p > 0.05)。在酸蚀试验中,Nb2O5对Maxxion R和体外Fil R没有影响(p > 0.05)。Nb2O5添加量为10%时,体外磨牙酸蚀增加(p < 0.05)。Maxxion R为15.78 μm,而Vitro Molar和Vitro Fil R分别为5.14 μm和6.18 μm。随着Nb2O5浓度的增加,各组放射线透明度均增加。离体磨牙和离体Fil R对至少1 mm铝无显著差异(p > 0.05)。结论:5 wt.% Nb2O5的加入对GICs的理化性能没有影响,并改善了其中一种胶结物的透光性。因此,这些材料适合进一步测试仿生再矿化性能。
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