Thermal degradation assessment of canola and olive oil using ultra-fast gas chromatography coupled with chemometrics.

IF 1.7 4区 化学 Q3 CHEMISTRY, MULTIDISCIPLINARY Monatshefte Fur Chemie Pub Date : 2017-01-01 Epub Date: 2017-07-01 DOI:10.1007/s00706-017-1968-y
Tomasz Majchrzak, Martyna Lubinska, Anna Różańska, Tomasz Dymerski, Jacek Gębicki, Jacek Namieśnik
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引用次数: 20

Abstract

Abstract: Oil blending is often used to enhance the properties of vegetable oils. The admixture of a more thermally stable oil makes the resulting blend more suitable for use in frying. A new method of quality assessment of vegetable oils used in frying is presented in this paper. In this method, ultra-fast gas chromatography coupled with flame ionization detector and chemometrics is employed. Principal component analysis was used for data processing. The results obtained with this method were compared with the results of the Rancimat test and sensory evaluation. It is demonstrated that the addition of olive oil improves the stability of rapeseed oil, and also changes its flavour and aroma profile. In addition, it was found that ultra-fast GC coupled with chemometrics is an effective tool for the assessment of the quality of edible oils. The proposed method does not require sample preparation, and the total time of analysis is less than 2 min.

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超快速气相色谱-化学计量学评价菜籽油和橄榄油的热降解。
摘要:调油是提高植物油性能的常用方法。一种更热稳定的油的混合物使所得到的混合物更适合用于油炸。提出了一种评价油炸用植物油质量的新方法。该方法采用超快速气相色谱法、火焰电离检测器和化学计量学相结合的方法。数据处理采用主成分分析。并将所得结果与ranimat试验和感官评定结果进行了比较。结果表明,橄榄油的加入提高了菜籽油的稳定性,并改变了菜籽油的风味和香气特征。此外,还发现超快速气相色谱与化学计量学相结合是评价食用油质量的有效工具。该方法不需要样品制备,分析总时间小于2分钟。
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来源期刊
Monatshefte Fur Chemie
Monatshefte Fur Chemie 化学-化学综合
CiteScore
3.70
自引率
5.60%
发文量
116
审稿时长
3.3 months
期刊介绍: "Monatshefte für Chemie/Chemical Monthly" was originally conceived as an Austrian journal of chemistry. It has evolved into an international journal covering all branches of chemistry. Featuring the most recent advances in research in analytical chemistry, biochemistry, inorganic, medicinal, organic, physical, structural, and theoretical chemistry, Chemical Monthly publishes refereed original papers and a section entitled "Short Communications". Reviews, symposia in print, and issues devoted to special fields will also be considered.
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