Methacrylic Acid-Acrylamide based ZnO Hydrogel Nanocomposite Assisted Photocatalytic Decolorization of Methylene Blue Dye

Q3 Pharmacology, Toxicology and Pharmaceutics International Journal of Pharmaceutical Quality Assurance Pub Date : 2023-06-25 DOI:10.25258/ijpqa.14.2.06
A. Alkaim, F. H. Abdulrazzak, Shaimaa M. Essa, Usama S. Altimari, Montather F. Ramadan, Aseel M. Aljeboree
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Abstract

In this research, preparation of methacrylic acid-acrylamide based ZnO hydrogel nanocomposite (MAA-AM)/ZnO hydrogel nanocomposite by way of co-polymerization via used acrylate acid (AA) (or acrylate salt) (AA) or methacrylic acid (MAA)) and acrylamide (AM). Nanocomposites based on acrylate are characterized via being hydrophilic and able to retain water. Nanocomposite properties were studied using different techniques (FE-SEM, TEM, and EDX). The photocatalytic degradation of methylene blue MB dye under different conditions was studied using nanocomposite like time of irradiation, mass of catalyst (MAA- AM)/ZnO hydrogel nanocomposite, initial MB dye concentration onto photocatalytic degradation and reactivation were studied. The result increases the photocatalytic degradation with the rise weight of catalyst (MAA- AM)/ZnO hydrogel nanocomposite range (0.1–0.25 g). Too, a decrease in photocatalytic degradation was observed with an increase in MB. Observed that after reuse, ((MAA- AM)/ZnO) nanocomposite hydrogel appear photocatalytic efficiency from of the use 1 to 6 cycle 87.88 to 58.87%, showing that ((MAA- AM)/ZnO hydrogel nanocomposite surface appear good stability.
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甲基丙烯酸-丙烯酰胺基ZnO水凝胶纳米复合材料对亚甲基蓝染料的光催化脱色
在本研究中,通过用过的丙烯酸(AA)(或丙烯酸酯)(AA)或甲基丙烯酸(MAA))和丙烯酰胺(AM)共聚,制备了基于甲基丙烯酸丙烯酰胺的ZnO水凝胶纳米复合材料(MAA-AM)/ZnO水凝胶纳米复合材料。基于丙烯酸酯的纳米复合材料的特征在于亲水性和能够保持水。使用不同的技术(FE-SEM、TEM和EDX)研究了纳米复合材料的性能。利用纳米复合材料,如辐照时间、催化剂(MAA-AM)/ZnO水凝胶纳米复合材料的质量、MB染料的初始浓度等,研究了不同条件下亚甲基蓝MB染料的光催化降解和再活化。结果表明,随着催化剂(MAA-AM)/ZnO水凝胶纳米复合材料重量的增加(0.1–0.25 g),光催化降解增加。同样,随着MB的增加,观察到光催化降解的减少。观察到重复使用后,((MAA-AM)/ZnO)纳米复合水凝胶在使用1至6个循环中表现出87.88至58.87%的光催化效率,表明((MAA-AM)/Zn O纳米复合水凝胶表面表现出良好的稳定性。
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来源期刊
International Journal of Pharmaceutical Quality Assurance
International Journal of Pharmaceutical Quality Assurance Pharmacology, Toxicology and Pharmaceutics-Pharmacology, Toxicology and Pharmaceutics (miscellaneous)
CiteScore
0.80
自引率
0.00%
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0
期刊介绍: INTERNATIONAL JOURNAL OF PHARMACEUTICAL QUALITY ASSURANCE is a quarterly international journal publishing the finest peer-reviewed research in the field of Pharmaceutical Quality Assurance and Pharmaceutical Analysis on the basis of its originality, importance, disciplinary interest, timeliness, accessibility, elegance, and surprising conclusions. IJPQA also provides rapid, authoritative, insightful and arresting news and interpretation of topical and coming trends affecting science, scientists and the wider public.
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