Extraction and characterization of nanofibrillated cellulose from yacon plant (Smallanthus sonchifolius) stems

IF 1 4区 化学 Q4 POLYMER SCIENCE Polimeros-ciencia E Tecnologia Pub Date : 2021-07-28 DOI:10.1590/0104-1428.09620
R. S. D. Sousa, A. S. D. Andrade, M. L. Masson
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Abstract

Abstract This study aimed to evaluate the process of cellulose extraction from yacon stem using combined pulping and bleaching processes to produce nanofibrillated cellulose (NFC). First, a chemical pulping process with NaOH was applied and, subsequently, the pulp obtained was bleached. From the chemical pulp (CP) bleached, NFC was obtained by the mechanical defibrillation in a colloidal grinder. Then, chemical composition, and infrared analysis of the pulps were performed. The pulping process showed a lower amount of extractives and lignin content, as a low yield and an excessively dark pulp. The CP bleached with NaClO2 showed the best results increased whiteness of the pulp. A suspension of NFC with fibers of 5-60 nm in diameter, high crystallinity index, and thermal stability was obtained. The results are promising and demonstrate the technical feasibility of obtaining NFC from yacon stems waste which is ideal to apply to other materials of the industry.
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矢车菊茎中纳米纤维纤维素的提取与表征
摘要本研究以雪莲果茎为原料,采用制浆和漂白联合工艺提取纤维素,制备纳米纤化纤维素(NFC)。首先,采用氢氧化钠化学制浆工艺,然后对得到的纸浆进行漂白。以漂白后的化学纸浆(CP)为原料,在胶体粉碎机中进行机械除颤,得到NFC。然后对纸浆进行了化学成分分析和红外分析。该制浆工艺表现出萃取剂用量和木质素含量较低,产率低,浆色过深。氯化钠漂白后的CP浆白度提高效果最好。得到了直径为5 ~ 60nm、结晶度高、热稳定性好的NFC悬浮液。实验结果表明,从雪莲茎废弃物中提取NFC具有良好的技术可行性,可应用于工业上的其他材料。
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来源期刊
Polimeros-ciencia E Tecnologia
Polimeros-ciencia E Tecnologia 化学-高分子科学
CiteScore
2.00
自引率
0.00%
发文量
14
审稿时长
6 months
期刊介绍: Polímeros is a quarterly publication of the Associação Brasileira de Polímeros - ABPol (Brazilian Polymer Association), which publishes Review Articles, Original Articles and Short Communications, disclosing advances in the knowledge of Polymer Science and Technology.
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