Beginner's Guide to Raman Spectroelectrochemistry for Electrocatalysis Study

IF 6.1 Q1 CHEMISTRY, MULTIDISCIPLINARY Chemistry methods : new approaches to solving problems in chemistry Pub Date : 2022-10-26 DOI:10.1002/cmtd.202200042
Dr. Weiran Zheng
{"title":"Beginner's Guide to Raman Spectroelectrochemistry for Electrocatalysis Study","authors":"Dr. Weiran Zheng","doi":"10.1002/cmtd.202200042","DOIUrl":null,"url":null,"abstract":"<p>The need for continuous observation of electrocatalytic processes under operating conditions has promoted the popularity of in situ techniques coupled with electrochemical tests. In situ Raman spectrometer coupled with electrochemistry (or Raman spectroelectrochemistry) is a powerful tool to provide real-time structural information related to the dynamic electrolyte/electrode interface. To make it more accessible among the electrocatalysis community, we provide an essential experimental guideline of in situ Raman spectroelectrochemistry to beginners. After the necessary background of the technical principle and primary applications, we focus on the experimental considerations, from electrode preparation, cell design, and laser parameters to the electrochemical sequence and data process. The recent efforts to make this technique more affordable are also highlighted. We hope this review can help beginners to understand and use Raman spectroelectrochemistry.</p>","PeriodicalId":72562,"journal":{"name":"Chemistry methods : new approaches to solving problems in chemistry","volume":null,"pages":null},"PeriodicalIF":6.1000,"publicationDate":"2022-10-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/cmtd.202200042","citationCount":"5","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Chemistry methods : new approaches to solving problems in chemistry","FirstCategoryId":"1085","ListUrlMain":"https://onlinelibrary.wiley.com/doi/10.1002/cmtd.202200042","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 5

Abstract

The need for continuous observation of electrocatalytic processes under operating conditions has promoted the popularity of in situ techniques coupled with electrochemical tests. In situ Raman spectrometer coupled with electrochemistry (or Raman spectroelectrochemistry) is a powerful tool to provide real-time structural information related to the dynamic electrolyte/electrode interface. To make it more accessible among the electrocatalysis community, we provide an essential experimental guideline of in situ Raman spectroelectrochemistry to beginners. After the necessary background of the technical principle and primary applications, we focus on the experimental considerations, from electrode preparation, cell design, and laser parameters to the electrochemical sequence and data process. The recent efforts to make this technique more affordable are also highlighted. We hope this review can help beginners to understand and use Raman spectroelectrochemistry.

Abstract Image

查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
初级指南拉曼光谱电化学电催化研究
在操作条件下对电催化过程进行连续观察的需要促进了与电化学测试相结合的现场技术的普及。原位拉曼光谱仪耦合电化学(或拉曼光谱电化学)是一个强大的工具,提供有关动态电解质/电极界面的实时结构信息。为了使它在电催化界更容易理解,我们为初学者提供了一个必不可少的原位拉曼光谱电化学实验指南。在介绍了技术原理和主要应用的必要背景之后,我们重点讨论了从电极制备、电池设计、激光参数到电化学顺序和数据处理的实验考虑。最近的努力,使这项技术更实惠也突出。我们希望这篇综述可以帮助初学者理解和使用拉曼光谱电化学。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
CiteScore
7.30
自引率
0.00%
发文量
0
期刊最新文献
Cover Feature: (Chem. Methods 10/2024) Cover Picture: (Chem. Methods 9/2024) Rescaling NMR for a Larger Deployment in Drug Discovery: Hyperpolarization and Benchtop NMR as Potential Game-Changers Insights into CO2 Diffusion on Zeolite 13X via Frequency Response Technique Cover Picture: (Chem. Methods 7-8/2024)
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1