Synthesis, Characterization and Investigation of Magnetic Properties of Co3O4/CoFe2O4 Nanocomposite Prepared by Calcination of [CO(SALEN)(PPH3)(H2O)]4[Fe(CN)6] and [Co(Salophen)(PPH3)(H2O)]4[Fe(CN)6] Binary Complex Salts
{"title":"Synthesis, Characterization and Investigation of Magnetic Properties of Co3O4/CoFe2O4 Nanocomposite Prepared by Calcination of [CO(SALEN)(PPH3)(H2O)]4[Fe(CN)6] and [Co(Salophen)(PPH3)(H2O)]4[Fe(CN)6] Binary Complex Salts","authors":"A. Kianfar, N. Eskandari, M. A. Arayesh","doi":"10.47176/jame.39.2.19821","DOIUrl":null,"url":null,"abstract":"In this research the synthesis of [Co(Salen)(PPh3)(H2O)]4[Fe(CN)6] and [Co(Salophen)(PPh3)(H2O)]4[Fe(CN)6] schiff base complexes was reported. Co3O4/CoFe2O4 magnetic nanoparticles were prepared by calcination of these complexes at 500, 550 and 600°C. Precursor complexes were identified by FT-IR and UV-Vis spectroscopy and their thermal behavior was studied via TG/DTA. Nanomagnetic samples were characterized by X-ray diffraction (XRD), Scanning Electron Microscopy * یکینورتکلا تسپ ،تابتاکم لوئسم : : akianfar@cc.iut.ac.ir D ow nl oa de d fr om ja m e. iu t.a c. ir at 3 :4 4 IR S T o n S un da y N ov em be r 22 nd 2 02 0","PeriodicalId":30992,"journal":{"name":"Journal of Advanced Materials in Engineering","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2020-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Advanced Materials in Engineering","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.47176/jame.39.2.19821","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
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Abstract
In this research the synthesis of [Co(Salen)(PPh3)(H2O)]4[Fe(CN)6] and [Co(Salophen)(PPh3)(H2O)]4[Fe(CN)6] schiff base complexes was reported. Co3O4/CoFe2O4 magnetic nanoparticles were prepared by calcination of these complexes at 500, 550 and 600°C. Precursor complexes were identified by FT-IR and UV-Vis spectroscopy and their thermal behavior was studied via TG/DTA. Nanomagnetic samples were characterized by X-ray diffraction (XRD), Scanning Electron Microscopy * یکینورتکلا تسپ ،تابتاکم لوئسم : : akianfar@cc.iut.ac.ir D ow nl oa de d fr om ja m e. iu t.a c. ir at 3 :4 4 IR S T o n S un da y N ov em be r 22 nd 2 02 0
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