Xiaoxia Shang, Weifeng Huang, Yueqian Fan, Haijuan Wu, Meijun Wang, L. Chang, Dongfeng Li, Zhihong Li
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引用次数: 0
Abstract
Abstract Wide-angle X-ray scattering (WAXS) based upon synchrotron radiation is ideal for the in situ study of crystal structural changes during heating at high temperatures. This contribution describes a small furnace for in situ WAXS. The furnace has a wide coverage of scattered/diffracted angle from 0 to 135°, heats samples from room temperature to 1000 °C at 20 °C/min, and is suitable for in situ WAXS and radial distribution function of materials. Temperature calibration and safety verification are provided. The use of the furnace is demonstrated by in situ WAXS for the carbonization of bituminous coal.
期刊介绍：
Instrumentation Science & Technology is an internationally acclaimed forum for fast publication of critical, peer reviewed manuscripts dealing with innovative instrument design and applications in chemistry, physics biotechnology and environmental science. Particular attention is given to state-of-the-art developments and their rapid communication to the scientific community.
Emphasis is on modern instrumental concepts, though not exclusively, including detectors, sensors, data acquisition and processing, instrument control, chromatography, electrochemistry, spectroscopy of all types, electrophoresis, radiometry, relaxation methods, thermal analysis, physical property measurements, surface physics, membrane technology, microcomputer design, chip-based processes, and more.
Readership includes everyone who uses instrumental techniques to conduct their research and development. They are chemists (organic, inorganic, physical, analytical, nuclear, quality control) biochemists, biotechnologists, engineers, and physicists in all of the instrumental disciplines mentioned above, in both the laboratory and chemical production environments. The journal is an important resource of instrument design and applications data.
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