Phenolic compounds from section Majorana (Mill.) Benth of Origanum L. species extracts via validated LC-MS/MS method

IF 1.8 Q3 CHEMISTRY, ANALYTICAL Journal of Chemical Metrology Pub Date : 2022-12-31 DOI:10.25135/jcm.80.2211.2667
S. Carikci, A. Gören, T. Kilic, T. Dirmenci
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Abstract

AbstrAbstract: Origanum majorana L., (OM), O. onites L. (OO) and O. syriacum L. (subsp. bevanii (Holmes) Greuter & Burdet) (OS) are belong to Majorana (Mill.) Benth. section of Origanum L. genus. In this study, quantities of some phenolic compounds; gallic acid, syringic acid, p -hydory benzoic acid, caffeic acid, ( E )-ferulic acid, chlorogenic acid, rosmarinic acid, pyrogallol and vanillin; in the chloroform (C), acetone (Ac) and methanol (M) extracts prepared from Origanum species collected from Türkiye were investigated via liquid chromatography and tandem mass spectrometry (LC-MS/MS). The relative standard deviations (RSD) of the phenolics were found as follows; 4.85, 8.39, 4.78, 8.04, 5.21, 5.45, 3.73, 5.47, respectively. Curcumin was used as an internal standard. In the extracts, ( E )-ferulic acid and caffeic acid were found to be the most abundant compounds. O. syriacum was determined as the richest species in terms of phenolic acids.
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通过验证的LC-MS/MS方法从牛至属植物Majorana(Mill.)Benth部分提取的酚类化合物
文章摘要:牛至(Origanum majorana L.)、(OM)、O.onites L.(OO)和O.syracum L.(subsp.bevanii(Holmes)Greuter&Burdet)(OS)属于majorana(Mill.)Benth。牛至属的一个部分。在本研究中,一些酚类化合物的数量;没食子酸、丁香酸、对羟基苯甲酸、咖啡酸、(E)-阿魏酸、绿原酸、迷迭香酸、邻苯三酚和香草醛;通过液相色谱和串联质谱(LC-MS/MS)研究了从土耳其采集的牛至属植物制备的氯仿(C)、丙酮(Ac)和甲醇(M)提取物。酚类化合物的相对标准偏差(RSD)如下:;分别为4.85、8.39、4.78、8.04、5.21、5.45、3.73、5.47。姜黄素被用作内标。提取物中,(E)-阿魏酸和咖啡酸含量最高。丁香被确定为酚酸含量最丰富的物种。
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来源期刊
Journal of Chemical Metrology
Journal of Chemical Metrology CHEMISTRY, ANALYTICAL-
CiteScore
2.30
自引率
15.40%
发文量
7
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