Surface Roughness, Hardness and FTIR of the Modified Soft Liner with Different Metal Oxide Nanoparticles

Mohammed M. Sadoon, A. Al-Noori
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Abstract

Aims: To study the effect of metal oxide nanoparticles (MgO, ZrO2, ZnO) on acrylic based soft liner surface properties and FTIR. Materials and Methods: Acrylic-based soft-liner specimens were prepared by adding three different concentrations (0.5, 1, and 2) %wt of metal oxide nanoparticles (MgO, ZrO2, ZnO). A disk-shaped specimens with 30mm diameter and 3mm thickness were prepared for shore (A) hardness test to evaluate the surface hardness of modified soft liner. The surface roughness of soft-liner samples (10X10X2mm) was tested by a profilometer. FTIR analysis was conducted to evaluate chemical reaction that may occur between acrylic-based soft liner and nanoparticles. Results : there were no chemical reaction carried out between soft liner and metal oxide nanoparticles at different concentration- surface hardness (shore A) was increased as nanoparticles concentration increased in modified resin. Nanoparticles with 1 and 2% concentration incorporated in soft liner had lower surface roughness value. Conclusions : Metal oxide nanoparticles have improved the surface texture of acrylic-based soft liner, while the hardness of modified soft liner was increased with nanoparticles concentration increases.
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不同金属氧化物纳米颗粒改性软衬的表面粗糙度、硬度和红外光谱
目的:研究金属氧化物纳米颗粒(MgO, ZrO2, ZnO)对丙烯酸基软衬表面性能和红外光谱的影响。材料和方法:通过添加三种不同浓度(0.5,1,2)%wt的金属氧化物纳米颗粒(MgO, ZrO2, ZnO)制备丙烯酸基软衬里样品。制备直径30mm、厚度3mm的圆盘状试样进行shore (A)硬度试验,评价改性软衬的表面硬度。采用轮廓仪对软衬样品(10X10X2mm)的表面粗糙度进行了测试。FTIR分析评价了丙烯酸基软衬里与纳米颗粒之间可能发生的化学反应。结果:不同浓度的金属氧化物纳米颗粒与软衬之间没有发生化学反应,改性树脂中纳米颗粒浓度越大,表面硬度(shore A)越高。在软衬中掺入浓度为1%和2%的纳米颗粒,其表面粗糙度值较低。结论:金属氧化物纳米颗粒改善了亚克力基软衬的表面质地,改性软衬的硬度随纳米颗粒浓度的增加而增加。
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发文量
34
审稿时长
10 weeks
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