Crystal Structure of [N-(9-Anthracenylmethyl)-1,3-propanediamine](2,2′-bipyridine)platinum(II) Chloride

IF 0.1 Q4 CRYSTALLOGRAPHY X-ray Structure Analysis Online Pub Date : 2019-07-10 DOI:10.2116/XRAYSTRUCT.35.39
T. Kiwada, H. Takayama, Hiromu Katakasu, A. Odani
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Abstract

The crystal structure of [ N -(9-anthracenylmethyl)-1,3-propanediamine](2,2 ′ -bipyridine)platinum(II) chloride was determined by X-ray crystallography. The title complex crystallized in the monoclinic space group P 21/ c and Z = 4 with cell parameters a = 11.2466(7)Å, b = 17.3553(10)Å, c = 13.7027(9)Å, β = 100.501(2) ° , V = 2629.8(3)Å 3 . [ I > 2 σ ( I )] and wR 2 (all data) values are 0.0271 and 0.0619, respectively, for all 5995 independent reflections. The intramolecular π-π stacking interaction was observed between the anthracene and the bipyridine. In the crystal packing structure, the intermolecular π-π stacking interaction was observed. 2019)
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[N-(9-蒽甲基)-1,3-丙二胺](2,2′-联吡啶)氯化铂(II)的晶体结构
用X射线晶体学方法测定了[N-(9-蒽甲基)-1,3-丙二胺](2,2′-联吡啶)氯化铂(II)的晶体结构。标题配合物在单斜空间群P21/c和Z=4中结晶,细胞参数a=12.466(7)Å,b=17.3553(10)Å、c=13.7027(9)Å和β=100.501(2)°,V=22629.8(3)Å3。对于所有5995个独立反射,[I>2σ(I)]和wR2(所有数据)值分别为0.0271和0.0619。蒽和联吡啶之间存在分子内π-π堆积相互作用。在晶体堆积结构中,观察到分子间π-π堆积相互作用。2019)
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0.60
自引率
50.00%
发文量
17
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