Diffusion and Thermal Shock Behaviour of Silicate Dental Ceramics

IF 0.8 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Science-medziagotyra Pub Date : 2023-02-24 DOI:10.5755/j02.ms.30414
B. Ertuğ
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Abstract

The purpose of this study is to examine the diffusion and thermal shock behaviour of the alternative dental silicates. The samples derived from BaO-SiO2 system have been produced by melting process and followed by the heat treatment. X-ray examinations have indicated that the amount of orthorhombic sanbornite phase rised due to treatment temperature as revealed by the peak intensities. The alteration of the morphology by treatment temperature was evident from scanning electron microscopy SEM images. Crystallization at low temperature produced small crystallites and coarsening was not observed with a rise in temperature. The failure of the dental samples after the thermal shock test was examined using SEM. A continuous crack geometry and very few crack branching were observed. Diffusivity constant (D) and diffusion rate were examined vs treatment temperature for the present system. Diffusion depth (L) was doubled when the crystallization treatment was applied. Based on the obtained results, these silicate samples might take part in the further characterization studies to be used as alternative dentistry materials.
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硅酸盐牙科陶瓷的扩散和热冲击行为
本研究的目的是研究替代牙科硅酸盐的扩散和热冲击行为。采用熔融法制备了BaO-SiO2体系样品,并对样品进行了热处理。x射线检查表明,由于处理温度的升高,正交三斑岩相的数量增加,如峰值强度所示。从扫描电镜(SEM)图像可以看出,处理温度对合金形貌的影响是明显的。低温结晶产生小晶粒,温度升高时未观察到粗化现象。用扫描电子显微镜观察热冲击试验后牙体试样的破坏情况。裂纹几何形状连续,裂纹分支极少。测定了该体系的扩散系数常数(D)和扩散速率随处理温度的变化。结晶处理使扩散深度(L)增加了一倍。基于所获得的结果,这些硅酸盐样品可能会参与进一步的表征研究,以用作替代牙科材料。
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来源期刊
Materials Science-medziagotyra
Materials Science-medziagotyra 工程技术-材料科学:综合
CiteScore
1.70
自引率
10.00%
发文量
92
审稿时长
6-12 weeks
期刊介绍: It covers the fields of materials science concerning with the traditional engineering materials as well as advanced materials and technologies aiming at the implementation and industry applications. The variety of materials under consideration, contributes to the cooperation of scientists working in applied physics, chemistry, materials science and different fields of engineering.
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