Glycolipids isolation and characterization from natural source: A review

IF 1 4区 化学 Q4 BIOCHEMICAL RESEARCH METHODS Journal of Liquid Chromatography & Related Technologies Pub Date : 2022-10-02 DOI:10.1080/10826076.2023.2165097
A. Daku, S. B. Al-Mhanna, Ruzilawati Abu Bakar, A. Nurul
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Abstract

Abstract For centuries, many natural products are known to contain a wide range of glycolipid compounds; some are chemical substances that produce a definite biological/physiological effect. Isolation and characterization of glycolipids are evolving with new techniques being or under development. This review gives a brief description of different methods of natural glycolipids extraction, isolation, and characterization. Modern extraction instruments and techniques accelerate glycolipids’ extraction processes. Chromatographic methods, such as column chromatography and TLC are the most commonly used techniques for glycolipid isolation and purification, different characterization techniques ranging from chemical methods, reagents spray UV-detection, MS, FTIR, and NMR with later tandem-MS, TOF, FID, ESI, and ELSD modifications of the existing techniques allowing faster, more sensitive and direct analysis. Graphical Abstract
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天然来源糖脂的分离与表征综述
几个世纪以来,许多天然产物被认为含有广泛的糖脂化合物;有些是产生一定生物/生理效应的化学物质。随着新技术的出现和发展,糖脂的分离和表征也在不断发展。本文综述了天然糖脂提取、分离和表征的不同方法。现代提取仪器和技术加速了糖脂的提取过程。色谱方法,如柱层析和薄层色谱是糖脂分离和纯化最常用的技术,不同的表征技术包括化学方法,试剂喷雾紫外检测,质谱,FTIR和NMR,以及后来的串联质谱,TOF, FID, ESI和ELSD对现有技术的修改,使分析更快,更敏感和更直接。图形抽象
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来源期刊
CiteScore
2.80
自引率
0.00%
发文量
29
审稿时长
4.9 months
期刊介绍: The Journal of Liquid Chromatography & Related Technologies is an internationally acclaimed forum for fast publication of critical, peer reviewed manuscripts dealing with analytical, preparative and process scale liquid chromatography and all of its related technologies, including TLC, capillary electrophoresis, capillary electrochromatography, supercritical fluid chromatography and extraction, field-flow technologies, affinity, and much more. New separation methodologies are added when they are developed. Papers dealing with research and development results, as well as critical reviews of important technologies, are published in the Journal.
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