An Eco-Friendly Synthesis of Silver Nanoparticles Using Extract of Capsicum chinense Jacq. as A Bio-reducing Agent

Boyfannie Ivan Putra, Hermin Sulistyarti, R. Retnowati, M. Rafi
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Abstract

Silver nanoparticles (AgNPs) have become popular due to their unique properties that can be used as biosensors, composite fibers, semiconductor materials, and other medical applications. Green synthesis of AgNPs using natural reagents from plant extract offers advantages as an efficient and environmentally friendly technique by which the compounds from the extract perform as bio-reductor for silver ions and the capping agent for stabilizing the AgNPs. Therefore, the purpose of the study was to conduct the synthesis of AgNPs by utilizing an extract of Capsicum chinensie Jacq as the bioreductor. The effect of extract concentrations, duration of exposure to sunlight, and temperatures on AgNPs formation was studied to obtain the optimum synthesis condition. The biosynthesized AgNPs characteristics were analyzed using UV-Vis Spectrophotometry, FTIR, SEM, X-Ray Diffraction, and PSA. The results showed that the higher extract concentration produced smaller AgNPs. The synthesis under sunlight exposure showed more product of AgNPs compared to heating on a hot plate. The optimum conditions of biosynthesis of AgNPs were attained at the volume ratio of extract (20%) and AgNO3 (1mM) of 1:1 and duration of sunlight exposure of 90 min, resulting in AgNPs characterized with maximum wavelength 422 nm and average particle sizes of 67.94 nm.
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利用辣椒提取物环保合成纳米银。作为生物还原剂
银纳米颗粒(AgNPs)因其独特的性能而广受欢迎,可用于生物传感器、复合纤维、半导体材料和其他医疗应用。使用来自植物提取物的天然试剂绿色合成AgNPs提供了作为一种有效和环境友好的技术的优势,通过该技术,来自提取物的化合物充当银离子的生物还原剂和用于稳定AgNPs的封端剂。因此,本研究的目的是利用辣椒提取物作为生物还原剂来合成AgNPs。研究了提取物浓度、暴露时间和温度对AgNPs形成的影响,以获得最佳合成条件。利用紫外-可见分光光度法、红外光谱、扫描电镜、X射线衍射和PSA分析了合成的AgNPs的特性。结果表明,提取物浓度越高,AgNPs越小。与在热板上加热相比,在阳光照射下的合成显示出更多的AgNPs产物。在提取液(20%)和硝酸银(1mM)的体积比为1:1、光照时间为90min的条件下,获得了AgNPs生物合成的最佳条件,得到了最大波长为422nm、平均粒径为67.94nm的AgNPs。
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发文量
36
审稿时长
17 weeks
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